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Document / 28 pages

GC/MS calibration table for TCLP analysis, Nov 2001

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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.

NYC-WTC_000069154–000069181

Folder label: “GCMS Scan X 10/19/01 An 11/8/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0801\LBA.D Vial: 8 Acq On : 8 Nov 2001 9:26 pm Operator: 209 GALOS Sample : 10/19 lab blk Inst ; GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 17 Hexatriacontane Concentration Rank 19 R.T. EstConc Area Relative to ISTD R.T. 39.51 0.43 ug/1 167795 Perylene-dl2 37.17

Hit# of 5 Tentative ID MW MolForm CAS# 1 Hexatriacontane 507 C36H74 000630-06-8(91/ 2 Tetratetracontane 619 C44H90 007098-22-8 87 3 Nonadecane, 9-methyl- 282 C20H42 013287-24-6 83 4 Heneicosane 296 C21H44 000629-94-7 81 Abundance Scan 3755 (39.513 min); LBA.D (-) m/z 56.95 100.00% 5|7

5000 85

, (1P14O 1931......... 281......................................................................... _3a20_3a40_3a60_3a8g_^_ vIXvaTyt* “m/z 43705 67.81% Ti/z-> 50I 100 150 200 250 300 350 400 450 500 550 600 Abundance #74636: Hexatriacontane 57

5000 85 ^.20 39.40 39.60 39.80 ■m/z 71.05 64.22%

Tl/Z-> 50 .f 100 150 200 .... 250 300 350 400 450 500 550 600 Abundance #74745: Tetratetracontane 57 ' I ' ' ' ' I 39.20 39.40 39.60 39.80 5000 85 “mTz 85.05 48.53%

........................................................ 4634915195y 591618 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #39865: Nonadecane, 9-methyl- 5|7 39,20 39.40 39.60 39.80 m/z 55.00 25.76% 85 553 140'168 1113

■n/z-> 50 ML . I 100 150 200 252282 250 300 350 400 450 500 550 600 39.20 39.40 39.60 39.80

LBA.D NP103001.M Mon Nov 19 14:43:56 2001 Page 17

NYC-WTC_000069176

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NYC-WTC_000069176Source: NYC Law Department, mirrored locally

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