GC/MS calibration table for TCLP analysis, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File s C:\HPCHEM\1\DATA\NOV0801\LBA.D Vial: 8 Acq On ; 8 Nov 2001 9:26 pm Operator: 209 GALOS Sample : 10/19 lab blk Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 18 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T. 39.63 0.58 ug/1 225595 Perylene-dl2 37.17 Hit# of 5 Tentajzj-ve ID MW MolForm CAS# Qual 1 3-Isopropox)^, 1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 25 2 Cyclopropaiiamine, N-methyl-1-phenyl 147 C10H13N 056771-48-3 22 3 1,2-Be: "enedicarboxylic acid, bis(t 310 C14H22O4Si2 002078-22-0 16 4 3,6-^oxa-2,4,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 16 Abundance Scan 3768 (39.633 min): LBA.D (-) m/z 73.00 100.00% 713 147

221 5000 281 ■««

39 , IRI I 2531 I [ 327^ I[ 429............................. 401J 39.40 39.60 39.80 40.00 I f I T r . . I I I r I J I I 1 V I I 1 J 1 f I . T I J . i i I I . . I I I I I m/z 147.0081.90% TtZZ-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503; 3-lsopropoxy-1.1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 "n • ' ' ’ I • ' ' ' r ' 147 39.40 39.60 39.80 40.00 m/z 221.05 57707% 221 281 097 ..c J I ........... y................ 519,561 Wz-> 50 100 150 260 2^ 300 350 400 450 500 ' ' 550 Abundance #9103: Cyclopropanamine, N-methyl-1-phenyl- 147

39.40 39.60 39.80 40.00 To m/z 281.00 25.15%

42 92 12q nfe-> 50 100 150 200 . 250 300 350 400 450 500 550 Abundance #72973:1,2-Benzenedicarboxylio acid, bis(trimethylsilyl) e 147 39.40 39.60 39.80 40.00 73 m/z 354.95 19.36%

5000

295 45 I T-r-j-r-r A ' ' I ■nZz-> 50 100 150 200 250 300 350 400 450 500 550 39.40 39.60 39.80 40.00

LBA.D NP103001.M Mon Nov 19 14:43:58 2001 Page 18

NYC-WTC_000069177