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Document / 28 pages

GC/MS calibration table for TCLP analysis, Nov 2001

Machine-extracted title · confidence 100%

Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.

NYC-WTC_000069154–000069181

Folder label: “GCMS Scan X 10/19/01 An 11/8/01

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Scanned page image, NYC-WTC_000069178
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\NOV0 8 01\LBA.D Vial: 8 Acq On 8 Nov 2001 9:26 pm Operator: 209 GALOS Sample 10/19 lab blk Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 19 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T.

41.58 0.62 ug/,1 240338 Perylene-dl2 37.17

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 Trisiloxanfe, 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 43 2 1,2-Benz^edicarboxylic acid, bis(t 310 C14H22O4Si2 002078-22-0 27 3 Mercapt^cetic acid, bis (trimethyls 236 C8H20O2SSi2 006398-62-5 17 4 Etham ■ioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 12 Abundance Scan 3980 (41.579 min): LBA.D (-) m/z 73.00 100.00% 73 147

221 5000 281 355 429 41 20 41.40 41.60 41.80 42.00 40 ,..96 117 ,, 193 rT- I' 11"’ 0'I I ‘' I . I I''" I'"' I' m/z 147.00 87.36% ■nfe-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #74103: Trisiloxane, 1,1,1,5.5,5-hexamethyl-3,3-bis[(trimet 73 147

. ■, ,, 1 5000 281 41 20 41.40 41.60 41.80 42.00 m/z 221.05 62723% 45 369

JL 117 297 249 . ' I" " I" " I''" I'" ‘ I" " I" " I i" " I I" " I ■nfe-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #72973:1,2-Benzenedicarboxylic acid. bis(trimethylsilyl) e 1 17

73 41 20 41.40 41.60 41.80 42.00 Til m/z 281.00 39702% 295 45 193 221 ......... i" " I" " I" " I'"' I' I ‘" J I" " I" " I" ‘' I" " I" " I P Tlfe-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #30949: Mercaptoacetic acid, bis(trimethylsilyl)- 73 4120 41.40 41.60 41.80 42.00 147 m/z 207.00 27754% 5000

221 45 I, ,, I '" I" " I" " I 104 . ... P"^ '' "1" " I'" 11 pTTTpTTTyrTTTpTTTyrTTTpT-TTpTT^^ P Tlfe-> 40 60 80 100120140160180200220240260280300320340360380400420 41.20 41.40 41.60 41.80 42.00

LBA.D NP103001.M Mon Nov 19 14:44:00 2001 Page 19

NYC-WTC_000069178

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NYC-WTC_000069178Source: NYC Law Department, mirrored locally

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