NYC-WTC_000086768
Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.995
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GC/MS calibration table for TCLP analysis, Nov 2001
Machine-extracted title · confidence 100%Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
NYC-WTC_000069154–000069181Folder label: “GCMS Scan X 10/19/01 An 11/8/01”
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NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\NOV0801\LBA.D Vial: 8 Acq On : 8 Nov 2001 9:26 pm Operator: 209 GALOS Sample : 10/19 lab blk Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 20 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 18 R.T. EstConc Area Relative to ISTD R.T. 44.03 0.49 ug/1 190133 Perylene-dl2 37.17 Hit# of .5 Tentative ID MW MolForm CAS# Qual 1 Tris^oxane, 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 35 2 3-I^propoxy-l,1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 25 3 l,^Benzenedicarboxylic acid, bis(t 310 C14H22O4Si2 002078-22-0 25 4 t»^rcaptoacetic acid, bis (trimethyls 236 C8H20O2SSi2 006398-62-5 17 ^bunij^nce Scan 4247 (44.030 min): LBA.D (-) m/z 73.00 100.00% 7i3 147 221
5000 281 355
3,9, 50 100 150 200 a 253 I 327 I I |il, iL 250 300 |i .1, I 350 401 T ' ' I ' I ' ' ' ' I ' ' ' ' i ' ' 400 450 500 550 43.60 43.80 44.00 44.20 44.40 m/z 147.00 84.38% Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 7P 147
5000 43.60 43.80 44.00 44.20 44.40 281 45 369 m/z 220.9567745% JU 1—r'-f-V-r' 117 207 249 , ' 250 ' ' 300 Tl/Z-> 50 100 150 200 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethy(-3,5,5-tris(trim 73
43.60 43.80 44.00 44,20 44.40 5000 m/z 281.00 32.59% 147
221 281 327 ........ ).... [ .... 415...... ^1 Tife-> 50 100 150 200 250 300 350 400 450 500 550 ^bundance #72973:1,2-Benzenedicarboxylic acid, bis(trimethylsilyl) e 1 17 43.60 43.80 44.00 44.20 44.40 73 m/z 206.95 27726% 5000
295 45 j L''''i_I ' 'I 119
nfe-> 50 100 150 200 250 300 350 400 450 500 550 43.60 43.80 44.00 44.20 44.40
LBA.D NP103001.M Mon Nov 19 14:44:03 2001 Page 2 0
NYC-WTC_000069179
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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Header page for a gas chromatography-mass spectrometry scan file related to environmental testing at the World Trade Center site.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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