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← Document results/DEP Box 21/GCMS X 11/20/01 A 11/26/01
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GCMS blank analysis results for sample AD28143, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.

NYC-WTC_000033707–000033722

Folder label: “GCMS X 11/20/01 A 11/26/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\NOV2 601\LBA.D vial: 9 Acq On 26 Nov 2001 6:31 pm Operator: 209 GALOS Sample 11/20 lab blk scan Inst GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

47.05 0.69 ug/1 133756 Perylene-d12 37.12

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Trisi loxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 35 2 1,2-B enzenedicarboxylic acid, bis(t 310 C14H22O4Si2 002078-22-0 35 3 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 12 4 3,8/Dioxa-2,9-disiladecane, 2,2,9, 9 234 C10H26O2Si2 018001-91-7 12 Abundance Scan 4576 (47.051 min): LBA.D (-) m/z 73.00 100.00% 73 147 221

5000 281 355

n/z-> .............. ...................... ,T, 40 60 80 100120140160180200220240260280300320340360380400420 46.80 47.00 47.20 47.40 m/z 147.00 77.27% .................. .................................... Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147

5000 46.80 47.00 47.20 47.40 281 m/z 220.95 70.88% 45 369 .......... / L 'I " ' 'I 117 207 249 'I'I "" I' -rq-r T TTTTTTTTTTTTTTTTT TTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTT m/z-> 40 60 80 100120140 160 180 200220 240260 280300 320 340 360 380 400 420 Abundance #72973:1,2-Benzenedicarboxylic acid, bis(trimethylsilyl) e 147 73 46.80 47.00 47.20 47.40 5000 m/z 281.00 36.42% */ 45 .295 119 , m .. —... — UI’ 193 2 TTUETITI’TTTTTTTTTT’ TT‘). nrp TCICTTIEIE‘TUTCTI‘‘‘‘T m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #30580: Ethanedioic acid, bis(trimethylsilyl) ester 73 147 46.80 47'00 47.20 47.40 m/z 354.95 34.18% ............ .............................. 5000 45

m/z—> m 190 219 mpmTTTTTTTTTTmTTTTTT TTTPTTTTTT 40 60 80 100120140160180200220240260280300320340360380400420 46.80 47.00 47.20 47.40

LBA.D GCMS1126.M Tue NOV 27 12:44:30 2001 Page 9

NYC-WTC_000033721

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Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

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