Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.
NYC-WTC_000033707–000033722Folder label: “GCMS X 11/20/01 A 11/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\NOV2 601\LBA.D Vial: 9 Acq On : 26 Nov 2001 6:31 pm Operator: 209 GALOS Sample : 11/20 lab bik scan Inst : GC/MS 209 Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.
43.97 1.89 ug/1 365657 Perylene-dl2 37.12
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 38 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 35 3 3-Is/propoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 28 4 Mercaptoacetic acid, bis (trimethyls 236 C8H20O2SSi2 006398-62-5 17 Abundance Scan 4240 (43.966 min): LBA.D (-) m/z 73.00 100.00% 73 147 221
5000 281 355 T 191 .. 429 43 60 43.80 44.00 44.20 44 117 ial ,3271. 401 i 1’ ’ r —*. r.1.+ - ■ i ■ ■ ' r I +—mI m/z 147.00 90.56%
.A ■ m/z—> 50 100 150 200 250 300 350 400 450 500 550 Abundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- 147 221
73 5000 43.60 43.80 44.00 44.20 191 m/z 221.05 70.30%
mz— > Abundance
5000 .Ll—— 50 73 100 150 279
200 250 300 350 400 450 500 550 #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis((trimet
147
281 .A. 43.60 43.80 44.00 44.20 m/z 281.00 31.09% '
m/z—> 45 117 TTITTIT 1 ' i ’ • 50 100 150 207 249 200 250 300 350 400 450 500 . 3.... .. 550 Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim ■ i ■ ■ ■ ■ i ■ ■ 1 ' i ■ ■ ■ ' । ■ • ■ • । ■ 73 43.60 43.80 44.00 44.20 m/z 207.00 27.95% 5000 147 AH 221 281 327 415 519 561 11111141 •11 ■ । ■1 i ‘ -....... I I T T T TiT m/z—> 50 100 . 150 200 250 300 350 400 450 500 550 43.60 43.80 44.00 44.20
LBA.D GCMS1126.M Tue NOV 27 12:44:28 2001 Page 8
NYC-WTC_000033720
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NYC-WTC_000033886
Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000030685
Header page for a gas chromatography-mass spectrometry scan file related to environmental testing at the World Trade Center site.
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Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033765
Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017663
Laboratory report documenting gas chromatography-mass spectrometry blank analysis conducted on December 27, 2001.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019049
Laboratory report documenting gas chromatography-mass spectrometry blank analysis for volatile organic compounds conducted on January 7, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034180
Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034331
Laboratory report documenting GCMS analysis of sample AD28427 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034830
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047955
GCMS blank analysis report for sample AE08209 listing volatile organic compounds from April 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034958
Calibration report showing recovery percentages for various chemical standards used in the GCMS analysis.
1 shared non-person entities · 1 shared topics · similarity 0.991
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NYC-WTC_000033704
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000033705
Fragmented page from a GCMS-related record dated between November 20 and 26, 2001, likely part of the WTC environmental monitoring series.
Filed in the same folder
NYC-WTC_000033723
Calibration record for GCMS instrument 209 using method GCMS1126, dated November 26-28, 2001, listing standard compounds and retention times.
Filed in the same folder
NYC-WTC_000033726
Laboratory report of a GCMS reference analysis for sample AD28143 conducted on November 28, 2001, listing detected compounds and retention times.
Filed in the same folder
NYC-WTC_000033731
Laboratory report detailing GCMS analysis of sample AD28145 conducted on November 29, 2001, noting unknown compounds.
Filed in the same folder