Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.
NYC-WTC_000033886–000033901Folder label: “GCMS X 11/20/01 A 11/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2 6 01\LBA.D Vial: 9 Acq On : 26 Nov 2001 6:31 pm Operator: 209 GALOS Sample : 11/20 lab bik scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 47.05 0.69 ug/1 133756 Perylene-dl2 37.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Trisiloxane, 1, 1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 35 2 1,2-Benzened /carboxylic acid, bis(t 310 C14H22O4Si2 002078-22-0 35 3 Ethanedioi acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 12 4 3,8-Dioxa4 ,9-disiladecane, 2,2,9,9 234 C10H26O2Si2 __ 018001-91-7 12 Abundance Scan 4576 (47.051 min): LBA.D (-) m/z 73.00 1 00.00% 73 147 221
5000 281 355 T
X 429 T ' I 1 • 191 I
miz-? 44 TT TTT 94 117 -234.44.. P" 40 60 80 100 120140160180200220240260280300320340360380400420 327+ 46.80 47.00 47.20 47.40 m/z 147.00 77.27% Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 -A---A---A-- , , , , , b , ----------- 5000
—A 281 46.80 47.00 47.20 47.40 45 369 m/z 220.95 70.88% t........ 117..... %............. 207 249 m/z->._ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420" Abundance #72972 1,2-Benzeneurcarboxylic acid, bis(trimethylsily)) e 147 73 5000
45 295 j 119 _ 193 221 | TTTg"TTTTTTnr TTTTTTTTTT AWW WWw miz-> 40 60 80 100120140160180200220 240 260 280300320340 360 380 400 420 Abundance #30580: Ethanedioic acid, bis(trimethylsilyl) ester 73 147 46.80 47.00 47.20 47.40 m/z 354.95 34.18% 5000 ............ / 45
I I 190 219 TTTTTTTTTTTTTTTT FTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTITTTTITTTTTTTTTT miz-> 40 60 80 100120140160180200220240260280300320340360380400420 46.80 47.00 47.20 47.40
LBA.D GCMS1126.M Thu Jan 03 12:52:42 2002 Page 9
NYC-WTC_000033900
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NYC-WTC_000033707
Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.
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Header page for a gas chromatography-mass spectrometry scan file related to environmental testing at the World Trade Center site.
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Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033765
Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017663
Laboratory report documenting gas chromatography-mass spectrometry blank analysis conducted on December 27, 2001.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019049
Laboratory report documenting gas chromatography-mass spectrometry blank analysis for volatile organic compounds conducted on January 7, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034180
Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034331
Laboratory report documenting GCMS analysis of sample AD28427 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047955
GCMS blank analysis report for sample AE08209 listing volatile organic compounds from April 2002.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034958
Calibration report showing recovery percentages for various chemical standards used in the GCMS analysis.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034830
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.991
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NYC-WTC_000033704
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
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NYC-WTC_000033705
Fragmented page from a GCMS-related record dated between November 20 and 26, 2001, likely part of the WTC environmental monitoring series.
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NYC-WTC_000033707
Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.
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NYC-WTC_000033723
Calibration record for GCMS instrument 209 using method GCMS1126, dated November 26-28, 2001, listing standard compounds and retention times.
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NYC-WTC_000033726
Laboratory report of a GCMS reference analysis for sample AD28143 conducted on November 28, 2001, listing detected compounds and retention times.
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