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GCMS analysis results for sample AD25259, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD25259 conducted on November 28, 2001, noting unknown compounds.

NYC-WTC_000069519–000069529

Folder label: “GCMS Scan X 10/24/01 An 11/9/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1401\25156.D Vial: 2 Acq On : 14 Nov 2001 5:36 pm Operator: 209 GALOS Sample : gc/ms unknown Inst s GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 41.58 0.45 ug/1 82750 Perylene-dl2 37.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Trisiloxan^ 1,1,1,5,5,5 -hexamethyl 384 C12H36O4Si5 003555-47-3 25 2 Mercaptoiluetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 16 3 Silane, //f (1-methyl-1,3-propanediyl) 234 C10H26O2Si2 056771-47-2 14 4 1-Mono^:noleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 12 Abundance • * Scan 3980 (41.580 min): 25156.D (-) m/z 73.00 100.00% 7b 147 221 5000 281 40 LL rTTTpTnyfln|inl|ii

40 60 80 100120140160180200220240260280a)0320340360380400420 429 _4I^_4L40_4t60_4t80_42^ m/z 146.95 83?^ Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3.3-bisI(trimet 73 147

5000 41 41.40 4l!6b' 41 & ‘^00 281 m/z 221.00 64.15% LX T...... ..a pUi|H«i|i/n| . I. . , , I , , . . I , , , , I . Tife-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #30949: Mercaptoacefic acid, bis(trimethylsilyl)- 713 147 41.20 41.40 41.60 41.80 42.00 5000 m/z 207.00 51.60% 221 45 193 TpTTTpIrTprr/pJrpTr ■mrpTnr TprrrjTTTTJTTTTpTrTT^^ Tife-> 40 60 80 100120140160180^)0220240260280300320340360380400420 ^bunda^ce #71023: Silane, [(1-methyi-1,3-propanediyl)bis(oxy)]bis[tri Tb 147 41.20 41.40 41,60 41.80 42.00 m/z 281.00 32.39% 117 5000

Tife-> uU t .T 219 .1^,11 ,,. |i,,, I

40 60 80 1001201401601802002^)240260280300320340360380400420 41.20 41.40 41,60 41.80 42.00

25156.D NP103001.M Wed Nov 28 12:40:03 2001 Page 2

NYC-WTC_000069528

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NYC-WTC_000069528Source: NYC Law Department, mirrored locally

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