NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\NOV1401\25156.D Vial: 2
Acq On : 14 Nov 2001 5:36 pm Operator: 209 GALOS
Sample : gc/ms unknown Inst s GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
Peak Number 2 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
41.58 0.45 ug/1 82750 Perylene-dl2 37.16
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxan^ 1,1,1,5,5,5 -hexamethyl 384 C12H36O4Si5 003555-47-3 25
2 Mercaptoiluetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 16
3 Silane, //f (1-methyl-1,3-propanediyl) 234 C10H26O2Si2 056771-47-2 14
4 1-Mono^:noleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 12
Abundance • * Scan 3980 (41.580 min): 25156.D (-) m/z 73.00 100.00%
7b 147
221
5000
281
40
LL rTTTpTnyfln|inl|ii
40 60 80 100120140160180200220240260280a)0320340360380400420
429 _4I^_4L40_4t60_4t80_42^
m/z 146.95 83?^
Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3.3-bisI(trimet
73
147
5000 41 41.40 4l!6b' 41 & ‘^00
281
m/z 221.00 64.15%
LX T......
..a
pUi|H«i|i/n| . I. . , , I , , . . I , , , , I .
Tife-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #30949: Mercaptoacefic acid, bis(trimethylsilyl)-
713
147
41.20 41.40 41.60 41.80 42.00
5000 m/z 207.00 51.60%
221
45
193
TpTTTpIrTprr/pJrpTr
■mrpTnr TprrrjTTTTJTTTTpTrTT^^
Tife-> 40 60 80 100120140160180^)0220240260280300320340360380400420
^bunda^ce #71023: Silane, [(1-methyi-1,3-propanediyl)bis(oxy)]bis[tri
Tb 147 41.20 41.40 41,60 41.80 42.00
m/z 281.00 32.39%
117
5000
Tife->
uU t
.T 219 .1^,11 ,,. |i,,, I
40 60 80 1001201401601802002^)240260280300320340360380400420 41.20 41.40 41,60 41.80 42.00
25156.D NP103001.M Wed Nov 28 12:40:03 2001 Page 2
NYC-WTC_000069528
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