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Document / 28 pages

GC/MS calibration table for TCLP analysis, Nov 2001

Machine-extracted title · confidence 100%

Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.

NYC-WTC_000069154–000069181

Folder label: “GCMS Scan X 10/19/01 An 11/8/01

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Scanned page image, NYC-WTC_000069175
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV0 8 01\LBA.D Vial: 8 Acq On 8 Nov 2001 9:26 pm Operator: 209 GALOS Sample 10/19 lab blk Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 16 Heneicosane Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 38.28 0.66 ug/1 256817 Perylene-dl2 37.17 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91 2 Tetratetracontane 619 C44H90 007098-22-8 91 3 Hexatriacontane 507 C36H74 000630-06-8 91 4 Octadecane 254 C18H38 000593-45-3 91 Abundance Scan 3621 (38.283 min): LBA.D (-) in/z 57.00 100.00% 57

Saw 85

If , 253281 . . ,,,,,,,,,..... m/z 38.00 38.20 38.40 38.60 71.05 74707% ' ' I ' tUz-> 50 100 150 200 250 300 350 400 S) 5^' 600' Abundance #42201: Heneicosane 57

85 553 38.00 38.20 38.40 38.60 m/z 43.05 64.08% 113, h ,..................... 268296 ,, .................................................. r-n-p-r Tl/Z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #61068: Tetratetracontane 57

38.00 38.20 38.40 38.60 5000 “m/z 85.00 49.13% 85

I fr,''41irai97225 379407 590618 ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ■n/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #74636: Hexatriacontane 57 38.00 38.20 38.40 38.60 “Wz 55.00 27.76%

5000 85

jfj^w]4^?l^^r-r-r-rT-r-r-rn-p-rT-rTT-r-r^^

50 100 150 200 250 300 350 400 450 500 550 600 38.00 38.20 38.40 38.60

LBA.D NP103001.M Mon Nov 19 14:43:53 2001 Page 16

NYC-WTC_000069175

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NYC-WTC_000069175Source: NYC Law Department, mirrored locally

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