NYC-WTC_000086768
Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.995
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GC/MS calibration table for TCLP analysis, Nov 2001
Machine-extracted title · confidence 100%Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
NYC-WTC_000069154–000069181Folder label: “GCMS Scan X 10/19/01 An 11/8/01”
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NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOVO 8 01\LBA.D vial: 8 Acq On 8 Nov 2001 9:26 pm Operator: 209 GALOS Sample 10/19 lab blk Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 20 R.T. EstConc Area Relative to ISTD R.T. 38.06 0.42 ug/1 164065 Perylene-dl2 37.17 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 3,6-Dioxa-2,4y5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 40 2 EthanedioicU^id, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 17 3 2,6-DimethyT-3,4-bis(trimethylsilyl 311 C15H29NO2Si2 000000-00-0 12 4 3,7-Diox. 2,8-disilanonane, 2,2,8,8 220 C9H24O2Si2 017887-80-8 12 Abundance Scan 3597 (38.063 min): LBA.D (-) m/z 73.00 100.00% 73 147
221 5000 281 355 429 37.80 38.00 38.20 38.40 41 97 125 191 I 327 I ,.... 401 I TqhT-r-rYTT m/z 147.00 73.44%
K tt/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- 1 17 Z!1
73 5000 _3Y8O_3aog_^zo_^a4o_ 191 m/z 221.05 53.96% 117 279 I I P Tlfe-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #71006: Ethanedioic acid, bis(trimethylsilyl) ester 73 i I I I I
147 37.60 38-00 38.20 38.40 5000
45 117 190 219 I" " I"'' I"'' I r v/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #44359:2,6-Dimethyl-3,4-bis(trimethylsilyloxymethyl)pyridi Z!1 37.80 38.00 38.20 38.40 73 m/z 206.95 28757%
5000 147
m/z-> 45 .4^ Ju J................ 296...................................... '' I' 1111" " I" " I"' 11" " I'"' I'''' I" " I" " I" " I ‘' I' 40 60 80 100 120140160180 200 220 240 260 280 300 320 340 360 380 400 420 37.80 38.00 38.20 38.40
LBA.D NP103001.M Mon Nov 19 14:43:51 2001 Page 15
NYC-WTC_000069174
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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Header page for a gas chromatography-mass spectrometry scan file related to environmental testing at the World Trade Center site.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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