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GC/MS calibration table for TCLP analysis, Nov 2001

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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.

NYC-WTC_000069154–000069181

Folder label: “GCMS Scan X 10/19/01 An 11/8/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C;\HPCHEM\1\DATA\NOV0801\LBA.D Vial: 8 Acg On 8 Nov 2001 9:26 pm Operator: 209 GALOS Sample : 10/19 lab blk Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Eicosane Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 36.30 2.83 ug/1 1104870 Perylene-dl2 37.17 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 91 2 Hexatriacontane 507 C36H74 000630-06-8 91' 3 Heneicosane 296 C21H44 000629-94-7 90 4 Tetracosane 338 C24H50 000646-31-1 90 Abundance Scan 3405 (36.300 min); LBA.D (-) m/z 57.00 100.00% 5|7

85 5000

J J ^5 267 295 323 351 408 m/z 36.00 36,20 36,40 36,60 71.00 67.12% Ti/z-> 50 100 150 200 250 300 350 '460 ' ’ 450 ' ' '560 Abundance #39862; Eicosane 7

85 , , , 7 , , , , , , 5000 36,00 36,20 36,40 36,60 m/z 43.05 64.04% 196 2^ , ,282 50 100 150 200 250 300 3^^ 400^ 450 500 iKbundance #59136: Hexatriacontane 57 J V H ' ' ' I 36,00 36,20 36,40 36,60 5000 m/z 85.05 51.31% 85

_ 239 379 407 435 ■^8 506 ' ' I mfe-> 50 100 150 200 250 300 350 400 450 500 Abundance #42201: Heneicosane 7 36,00 36,20 36,40 36,60 m/z 557c 0 23,77% 85 5000

Ills V 100 \, 'h150 I...................................... V. ,,,200 2^ 300 400 ^0 500 Tlfe-> 50 36,00 36,20 36,40 36,60

LBA.D NP103001.M Mon Nov 19 14:43:49 2001 Page 14

NYC-WTC_000069173

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NYC-WTC_000069173Source: NYC Law Department, mirrored locally

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