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Document / 28 pages

GC/MS calibration table for TCLP analysis, Nov 2001

Machine-extracted title · confidence 100%

Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.

NYC-WTC_000069154–000069181

Folder label: “GCMS Scan X 10/19/01 An 11/8/01

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Scanned page image, NYC-WTC_000069172
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C;\HPCHEM\1\DATA\NOV0801\LBA.D Vial: 8 Acq On : 8 Nov 2001 9:26 pm Operator: 209 GALOS Sample : 10/19 lab blk Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Tridecane, 7-hexyl- Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 35.45 4.49 ug/1 1752510 Perylene-dl2 37.17 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tridecane, 7-hexyl- 268 C19H40 007225-66-3 2 Heneicosane 296 C21H44 000629-94-7 3 Octadecane 254 C18H38 000593-45-3 91 4 Heptacosane 380 C27H56 000593-49-7 91 Abundance Scan 3312 (35.446 min); LBA.D (-) m/z 57.00 100.00% 517

85 253

35.20 35.40 35.60 35.80 i I 141 169 197 225 253 281 309 337 365 394 m7z 71705 71.35% 1' ‘ " I ’'' ‘ p " ' I " " I' 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 /Sibundance #37464: Tridecane, 7-hexyl- 5f7

5000 85 35.20 35.40 35.60 35.80 182 m/z 43.00 66.98% I il 141 [l 268 TpnVryTTTTyrTnyrtTTYTTTYpnrTTjTrTTpTTTynTTyrTTTyTTTTjTTTTprTTTpTTTyrTTTp-^^ Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #42201; Heneicosane 57

85 35.20 35.40 35.60 35.80 5000 m/z 85.05 53.35% I I 113 4,14 268 296 I' « I • I H I I I k III 1 III II I I .. I" " I " ' ’ I I I r I [ I < I 11 I I . I 11 rmp ... I 11 < < I TTfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #71561: Octadecane 57 35.20 35.40 35.60 35.80 m7z 41.05 23.46% 85 5000

224 254 I " " I' ‘ " p'' ‘ I “ ' • I ‘ ' I F' “ P " ' P ‘ " P " ' P " ' I v •nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 35.20 35.40 35.60 35.80

LBA.D NP103001.M Mon Nov 19 14:43:47 2001 Page 13

NYC-WTC_000069172

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NYC-WTC_000069172Source: NYC Law Department, mirrored locally

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