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Document / 28 pages

GC/MS calibration table for TCLP analysis, Nov 2001

Machine-extracted title · confidence 100%

Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.

NYC-WTC_000069154–000069181

Folder label: “GCMS Scan X 10/19/01 An 11/8/01

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Scanned page image, NYC-WTC_000069171
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0801\LBA.D Vial: 8 Acq On : 8 Nov 2001 9:26 pm Operator: 209 GALOS Sample : 10/19 lab blk Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Pentadecane, 8-hexyl- Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T, 34.56 4.90 ug/1 2065290 Chrysene-dl2 33.07 Hit# of 5

p Tentative ID MW MolForm CAS# 1 Pentadecane, 8-hexyl- 296 C21H44 013475-75-7 2 Tridecane, 7-hexyl- 268 C19H40 007225-66-3 3 Eicosane, 10-methyl- 296 C21H44 054833-23-7 93 4 Heneicosane 296 C21H44 000629-94-7 91 Abundance Scan 3215 (34.556 min): LBA.D (-) m/z 57

85 slw! 4

TTfe-> 40 J ttYI 60 197 225 yTTTTp-TTTyTTT-rpTmyrTTTpT^ 253 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 295 323 351 380 I'''' I'''' I 34.20 34.40 34.60 34.80 m/z 71.10 72.06% Abundance #42199: Pentadecane, 8-hexyl- 413 71 / 5000 I ' ' ’ ' I 34.20 34.40 34.60 34.80

196 m/z 43.05 68.84% I1 I ,1 127 I , 266 296___________ r ‘' 'I"' ‘ I " " I I'''' I'''' I'''' I'' " I' ’'' I ‘‘ I'''' I Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #37464: Tridecane, 7-hexyl- 57 / V.................. 34.20 34.40 34.60 34.80 5000 85 54.04% 182

I Il 240 268 I II 11j 1 ill I n 11J11 ' I ’ ” ' p ' •«I • " • I' ’ • ri iTi I I" "I ""I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #42197: Eicosane, 10-methyl- 5|7 34.20 34.40 34.60 34.80 m/z 41.05 24.19% 5000 85

I 1 154

■nfe-> JULU t 268 296 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 I " “ I'''' I 34.20 34.40 34.60 34.80

LBA.D NP103001.M Mon Nov 19 14:43:44 2001 Page 12

NYC-WTC_000069171

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NYC-WTC_000069171Source: NYC Law Department, mirrored locally

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