GC/MS calibration table for TCLP analysis, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\NOV0801\LBA.D Vial: 8 Acq On : 8 Nov 2001 9:26 pm Operator; 209 GALOS Sample : 10/19 lab blk Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method s C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Tridecane, 7-hexyl- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 33.63 6.81 ug/1 2869430 Chrysene-dl2 33.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Tridecane, 7-hexyl- 268 C19H40 007225-66-3 9-3 2 Octadecane 254 C18H38 000593-45-3 9X 3 Heneicosane 296 C21H44 000629-94-7 91 4 Heptadecane 240 C17H36 000629-78-7 91 Abundance Scan 3114 (33.629 min): LBA.D {-) m/z 57700 100.00% 5|7

85 5000 / 4-

■n/z-> JXj J 40 |l'l, '*7 "I tJT“Trf 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 281 309 337 366 33.20 33.40 33.60 33.80 34.00 ~m7z 71710 70794% Abundance #37464: Tridecane, 7-hexyl- 57

5000 85 33,20 33.40 33.60 33,80 34.00 182 m/z 43.05 68.27% TTT-p yn-T I 240 268 iYrTThyrrTT]h-TTTy X. ' I' " ' I " " I'' I '' ‘' I " '' I " " I I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #71561: Octadecane 57 Ji ' ' I ' ' -p-r-r-r-p-r 33.20 33.40 33.60 33.80 34.00 85 5000 “m/z 85700 5^747%

, I ^^3 141 224 . ' I' ‘' I'''' I n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #42201: Heneicosane 57 33120 33.40 33.60 33.80 34.00 “m/z 41705 24791% 85 553

T)fe-> 40 I 113 44.4 ji,,i,,,Lj,i,i,, J......................... I'''' I'''' r ''' I'''' I'''' I' ’'' I' ’' * 1'' ’ I ‘' n 268 296 I " " I'''' I' 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 I' ‘ " I " " I J 33.20 33.40 33.60 33.80 34.00

LBA.D NP103001.M Mon Nov 19 14:43:42 2001 Page 11

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