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GC/MS calibration table for TCLP analysis, Oct 2001

Machine-extracted title · confidence 95%

Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.

NYC-WTC_000086768–000086785

Folder label: “508 Scan

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Scanned page image, NYC-WTC_000086781
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NYC 9/11 Public Portal Document Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT0101\LBA.D Vial: 2 Acq On 1 Oct 2001 2:41 pm Operator: 209 GALOS Sample 9/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ************************5*********************************************

Peak Number 8 Octadecane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 33.72 1.29 ug/1 292911 Chrysene-dl2 33.17 Hit# of 5 Tentative ID MW MolForm CAS# Qnal

1 Octadecane 254 C18H38 000593-45-3 91 2 Heneicosane 296 C21H44 000629-94-7 91 3 Eicosane 282 C20H42 000112-95-8 91 4 Tetratetracontane 619 C44H90 007098-22-8 91 Abundance Scan 3124 (33.717 min); LBA.D (-) m/z 56.95 100.00% 57 71 43 5000 85

__ I ----- r“n^-rT-rTT<Tr>p-T-rT-rT-'-r^ 113 ^.40 33.60 33.80 34.00

mfe-> 40 60 |4. 100 120 140 160 180 200 220 240 260 280 80 281 300 m/z 71.10 71709% ^bundance #71561: Octadecane 57 43 71 85 5000 ^.40 33.60 33.80 34.00 m/z 43.05 62784%

u 99 224 254 A 'I''"' I'''' I'''' I I ''' ' I ' ' '' I nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42201: Heneicosane 5(7 71 17 r. I . I I I 11 ........

85 33.40 33.60 33,80 34.00 5000 m/z 85.00 47765%

99 268 296 '' I ' ' ' I I' ’ ‘ I ’ ' ' 'I ■ ■ T . I . I I . I . I . I I I'' ■ 11 ■ ■ ■ 11' ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #72326: Eicosane 57 33.40 33.60 33.80 34.00 43 m/z 41.00 23790% 71 5000 85

99 iri J 127 141 155169 1 I . 1 I .’I . 1 . . l"» . • 1 I I i . 1 I'''' I'''' I'''' I 282 I__ nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 '33!4O 33^60 'ss'sO '34'00'

LBA.D NP091101.M Tue Oct 02 12:02:51 2001 Page 8

NYC-WTC_000086781

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NYC-WTC_000086781Source: NYC Law Department, mirrored locally

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