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GC/MS calibration table for TCLP analysis, Oct 2001

Machine-extracted title · confidence 95%

Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.

NYC-WTC_000086768–000086785

Folder label: “508 Scan”

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Scanned page image, NYC-WTC_000086780
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0101 \LBA.D Vial: 2 Acq On 1 Oct 2001 2:41 pm Operator: 209 GALOi Sample 9/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Tetracosane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 32.76 1.02 ug/1 231309 Chrysene-dl2 33.17 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane 338 C24H50 000646-31-1 91 2 Heneicosane 296 C21H44 000629-94-7 91 3 Heptadecane, 9-octyl- 352 C25H52 007225-64-1 91 4 Nonadecane, 2-methyl-____________ 282 C20H42 001560-86-7 91 Abundance Scan 3020 (32.762 min): LBA.D (-) m/z 56.95 100.00% 57

253 85

4 .1 1 J J iJ .1 . ISO 197 239 32.40 32.60 32.80 33.00 't ly*! I n*| rnn j^t i l*| i iTt-i-ri 11 f fnVj i P» i p i i i' । i i i i p*! i i ] i i > fpn » » | » i ri | » » i rpt t'» t ।» i i fp m/z 71.00 69.68% TiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 57

103 85 T 32.40 32.60 32.80 33.00 m/z 43.00 67.65% 294 338 T’rTyrTTTy-rTVTp^rTTyrTrrpd’TTyYTTrp-myTTTTpTT^^ TiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201: Heneicosane

85 32.40 32.60 32.80 33.00 5000 m/z 85.05 47754%

'' I'' ■n&-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #49558: Heptadecane, 9-octyl- V T 57 32.40 32.60 32.80 33.00 m/z 41.00 2^797%

5000 85

239 L 310 352 I . . . . |K.-.Yl .... I I ' '' r I' • ‘ ' I nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.40 32.60 32.80 33.00

LBA.D NP091101.M Tue Oct 02 12:02:49 2001 Page 7

NYC-WTC_000086780

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NYC-WTC_000086780Source: NYC Law Department, mirrored locally

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