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GC/MS calibration table for TCLP analysis, Oct 2001

Machine-extracted title · confidence 95%

Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.

NYC-WTC_000086768–000086785

Folder label: “508 Scan

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Scanned page image, NYC-WTC_000086779
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCTO101\LBA.D Vial: 2 Acq On 1 Oct 2001 2:41 pm Operator: 2 09 GTkLO; Sample 9/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Tetracosane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.77 0.99 ug/1 225543 Chrysene-dl2 33.17 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

Tetracosane 338 C24H50 000646-31-1 99 2 Eicosane 282 C20H42 000112-95-8 91 3 Octadecane 254 C18H38 000593-45-3 91 4 Heneicosane 296 C21H44 000629-94-7 91 Abundance Scan 2912 (31.771 min): LBA.D (-) m/z 57.00 100.00% 57 43 71

5000 85

Tife-> XU 40 60 99 ■Ji, J 281 338 I I fl I r| I .Ti I .1 I I fri II I 1.1. I'l I I Fl. I I < I ■ I ■ > I I < > 11 < I I ' I' " ' I'''' I " '' I'' 80 100 120 140 160 180 200 220 240 260 280 300 320 340 3Y4p 3Y60 31jg3Z00 32^ m/z71.00 72.69% Abundance #73543; Tetracosane 43 57 71

5000 85 3140 31.60 31.80 32.00 32.20 m/z 43.05 70.69% 155169183197 294 338 pn-iVp-lhTTrn-rn-r I " ' ‘ I TTTTTj-rTTTyrrTTy Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #39862: Eicosane 43 57

71 3140 31.60 31.80 32.00 32.20 5000 85 m/z 85.05 48.07%

'' I 11.1., T >. ■ I.. r I, I. i' I.. , 1. 111.. 1111.. 11111.1.11.,... I fl I ' I'''' I ‘ ‘ nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71561: Octadecane ...... ................ 57 31 40 31.60 31.80 32.00 32.20 43 71 m/z 41700 27741% 85 5000

1^,, .^1.TpL 224 2^ • I'' ‘ ’ I'' ” I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00 32.20

LBA.D NP091101.M Tue Oct 02 12:02:47 2001 Page 6

NYC-WTC_d00086779

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NYC-WTC_000086779Source: NYC Law Department, mirrored locally

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