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Document / 28 pages

GC/MS calibration table for TCLP analysis, Nov 2001

Machine-extracted title · confidence 100%

Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.

NYC-WTC_000069154–000069181

Folder label: “GCMS Scan X 10/19/01 An 11/8/01

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Scanned page image, NYC-WTC_000069165
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0801\LBA.D Vial: 8 Acq On 8 Nov 2001 9:26 pm Operator: 209 GALOS Sample 10/19 lab blk Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Octadecane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T.

30.65 3.03 ug/1 1277850 Chirysene-dl2 33.07

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane 254 C18H38 000593-45-3 91 2 Heneicosane 296 C21H44 000629-94-7 91 3 Eicosane 282 C20H42 000112-95-8 91 4 Heptadecane 240 C17H36 000629-78-7 9X Abundance Scan 2789 (30.645 min): LBA.D {-) m/z 57.00 100.00%! 57 43 71 85 5000

I yy 99 30.40 30.60 30.80 31.00 m/z 71.10 69.05% Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #71561: Octadecane 57 43 71

550 85 / V I ' ' ' 'I 30.40 30.60 30.80 31.00 99 m/z 43.05 66.03%

Tlfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #42201: Heneicosane 57 71 85 30.40 30.60 30.80 31.00 5000 m/z 85705 50.92% 99

' • ‘ ' I I ’ ' ' ' I ' ' ' 'I " r' I' " ■ I " " I ’ ' " I ’ ’ " I " ' • I • " ' I ‘ ' I " " I ' " ' I " ' ' I " n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #39862: Eicosane rI . . I . . . . f 43 5I7 30.40 30.60 30.80 31.00 71 m/z 41700 28.35%

5000 85

m&-> ' I ''' ' I '' 40 60 □u 113127141155 '' 1'''' I ' ' 240 282 196 I ' ' '' 1 ' 80 100 120 140 160 180 200 220 240 260 280 300 320 ' I ' ''' I'''' I'''' I'' '' I'''' I '' 1 T” 30.40 30.60 30.80 31.00

LBA.D NP103001.M Mon Nov 19 14:43:30 2001 Page 6

NYC-WTC_000069165

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NYC-WTC_000069165Source: NYC Law Department, mirrored locally

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