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GC/MS calibration table for TCLP analysis, Nov 2001

Machine-extracted title · confidence 100%

Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.

NYC-WTC_000069154–000069181

Folder label: “GCMS Scan X 10/19/01 An 11/8/01

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Scanned page image, NYC-WTC_000069166
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\NOV0801\LBA.D Vial: 8 Acq On : 8 Nov 2001 9:26 pm Operator: 209 GALOS Sample : 10/19 lab blk Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L A'**************************************************************'*****'*

Peak Number 7 Octadecanoic acid, 2-methylpro Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.

31.59 5.43 ug/1 2286690 Chrysene-dl2 33.07

Hit# of 5 Tentativi D MW MolForm CAS# Qual

1 Octadecanoic aci^ 2-methylpropyl e 340 C22H44O21 000646-13-9 66 2 Butyl tetradec^'oate (myristate) 284 C18H36O2I 000000-00-0 64 3 Octadecanoic ^id, butyl ester 340 C22H44O2i 000123-95-5 45 4 Cyclopropanxf 1-(1-methylethyl) -2-n 210 C15H30 041977-39-3 27 Abundance Scan 2892 (31.591 min): LBA.D (-) m/z 567^0 100.00% (1 5000 4- 73 129 285 340 31.20 31.40 31.60 31.80 32.00 0^ m/z 57.00 . 53.68% Tl/Z-> 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 5l7

5000 285 -JI„ 31.20 31.40 31.60 31.80 32.00 267 I m/z 43777 42.76%

" I' 7 1.7m?, 185 ('''' I'' ‘ 241 I. I I'l 11111'l 111 Pl I f' " ' [ 340 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 53 V 7^ 1 ' * ' ' I ' 31,20 31,40 31,60 31,80 32.00 5000 m/z 41.00 36.55% 229 73

■n&-> Abundance 40 60 §7191 I I 129 11'' 11''' 111''' I 185 I I'''' I'' ' JI 284 ' I'''' 11" ' I " " I " ' ’ I ”

80 100 120 140 160 180 200 220 240 260 280 300 320 340 #73570; Octadecanoic acid, butyl ester 31.20 31.40 31.60 31.80 32.00 m/z55700 32.62%

5000

73 129 267 285 340 A 185 I I'''' I'''' I I T-f fl . . I . . I I I '' I'''' I'' 'nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.20 31.40 31.60 31.80 32.00

LBA.D NP103001.M Mon Nov 19 14:43:33 2001 Page 7

NYC-WTC_000069166

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NYC-WTC_000069166Source: NYC Law Department, mirrored locally

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