GC/MS calibration table for TCLP analysis, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV0801\LBA.D Vial; 8 Acq On : 8 Nov 2001 9:26 pm Operator: 209 GALOS Sample : 10/19 lab blk Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library ; C:\DATABASE\NBS75K,L ********************************************************************* Peak Number 8 Tetracosane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 31.68 5.89 ug/1 2481710 Chrysene-dl2 33.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane 338 C24H50 000646-31-1 2 Tridecane, 7-hexyl- 268 C19H40 007225-66-3 93 3 Octadecane 254 C18H38 000593-45-3 91 4 Heptadecane 240 C17H36 000629-78-7 91 Abundance Scan 2902 (31.682 min); LBA.D {-) m/z 57.00 100.00%

43 5|7

71 A 85 5000

I 99 ' ~l I 1 Ji iJ \]^’’.F'’5'’''®51691831972112252^253267281295 31.40 31.60 31.80 32.00 338 I 1 p I ill I T l I p I I I I ri I'T I I ri I I p I I I I I f 1^1 I I "i I I I* I I 11 I I r I I I p I r I I I I I I I I I I I I I I I m/z 71705 68.90% nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 71

5000 85 ' I ' ' ' 31.40 31.60 31.80 32.00 99 mTz 43.05 65.49% ' I'' ‘ I I 11 111 11 I 11 I r I 11 'b t. i‘ 11 294 I ''' ' I '' ‘ ' I 338 ■"P" A TTfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #37464; Tridecane, 7-hexyl- 43 57 I ’ ‘'' I 71 31.40 31.60 31.80 32.00 5000 85 in/z 85.05 51.67% 182

240 268 n-ry-r I I' I'' I 1' I' I' I 7* ' ' I ' ' ' ' I ' ' n I ' ‘' I' ''' I ‘ ' I nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^bundance #71561: Octadecane 1^ 57 31.40 31.60 31.80 32.00 43 71 m/z 41.05 25.58% 85 5000

99 224 254 I I 11 I I T I I I I I I I I I I I > I I I I I I I ■ I I I I I I TT-p-rT-rp-T

40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31,40 31,60 31.80 32.00

LBA.D NP103001.M Mon Nov 19 14:43:35 2001 Page 8

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