GC/MS calibration table, Oct 1 2001

NYC 9/11 Public Portal Document

Library Search Compound- Report Data File : C:\HPCHEM\1\DATA\OCT3001\LB.D Vial: 8 Acq On : 30 Oct 2001 9:22 pm Operator: 209 GALOS Sample : lab blk 10/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P I

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************** Peak Number 6 Tetracosane Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 29.56 0.43 ug/1 119017 Chrysene-dl2 33.06 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane 338 C24H50 000646-31-1 9{) 2 Heneicosane 296 C21H44 000629-94-7 9o\ 3 Docosane 310 C22H46 000629-97-0 90/ 4 Heptadecane 240 C17H36 000629-78-7 86 Abundance Scan 2671 (29.565 min): LB.D (-) m/z 57700 100.00% 5|7 43 71 I A 85 5000

99 <| . .J \|^^?^141155169183197 29,20 29,40 29,60 29,80 MU r-^rTryry^KYrryrfTT-r^ryT^-rry'r-rTXYry-rryri-riyTi-rrYTTi-rYrTTTYrrrrYrT-rrYT m/z 43.05 71772% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 71

5000 85 29,20 29,40 29,60 29,80 99 m/z 71.10 70.02% J I, ,ii,, 294 338 I'''' I''' ‘ I'''' I I' ''' 1' tn/z-> 40 60 80 100 120 140-1160 180 200 220 240 260 280 300 320 340 Abundance #42201: Heneicosane

71 V A I ' ' • ' I 85 29.20 29,40 29,60 29,80 5000 m/z85.05 52.97% 99

I' '"' 1 ' ' '' I' ''' I '”’^“'“1 —---- —268 — 296 -|TTT-r-pTT-TyTTTT-prTT+j1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #44318: Docosane --T-p-T-rMMrMUrT^nVT-r 57— "29,20 ^29:40"”29,60^29,80'^-~‘ ~”71~” m/z 41.05 31.68% 85 5000

99

'' I'' ................ .................................... ................. r- nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 29 20 29 40 29 80 29 80

LB.D NP103001.M Mon Nov 05 08:56:58 2001 Page 6.

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