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GC/MS calibration table, Oct 1 2001

Machine-extracted title · confidence 100%

GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.

NYC-WTC_000089278–000089298

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089288
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NYC 9/11 Public Portal Document

Library Search Compound Report * Data File : C:\HPCHEiyi\l\DATA\OCT3001\LB.D Vial: 8 Acq On : 30 Oct 2001 9:22 pm Operator: 209 GALOS Sample : lab blk 10/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table ’ Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Butyl hexadecanoate Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 29.45 1.23 ug/1 339065 Chrysene-dl2 33.06 Hit# of 5 Tentative ID MW MolFdrm CAS# Qual

1 Butyl hexade panoate 312 C2 0H40O2 000000-00-0 35 2 1-Pentene ,/2 ,4-dimethyl- 98 C7H14 002213-32-3 27 3 Cyclobu^ .ne, 1,2 -diethyl - , trans- 112 C8H16 019341-98-1 27 4 1-Hex^^fie, 2-methyl- 98 C7Hi4" 006094-02-6 27 Abundance ' 53 Scan 2659 (29.455 min): LB.D (-) I ' I m/z 56.00 100.00%

5000 4 73 129 257 . . . I I . . . . lA Si "Of. n I I I . . I 143157171^ '. . . 312 29,20 29,40 29,60 29,80 +-T ■mTz 57700 49.00% nZz-> 20 40 60 80 100 120 .140 160 180 200 220 240 260 280 300 Abundance #44549: Butyl hexadecanoate 55

5000 258 -. 1 1 T, i-.-i -r|-. . ( . ,-r, 1 r. I 29,20 29,40 29,60 29,80 240 312, 129 m/^F 43705 39.78% ) I 1571711^ 214 ■ ,

I'''' I' TT+fTTTh-pHT-VYT"T+-fyrTH-rYrT-TTYrTVTyThT^^ ' I'''' I'' TiZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #63263:1-Pentene, 2,4-dimethyl- 53

‘ ' I ' ' ' ' I ' ■ .. 29,20 29,40 29,60 29,80 4 5000- m/z 41.05 34.56% 27 J ’l 98 ' I _ _ __ ' I ' ' ' ' I ' ' ' ‘ I ' ' ' ' I ' ' ‘ H ‘ ' I I ' ' ' ' I ' ' ' ' I ' ' ' ' I ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #2701: Cyclobutane, 1,2-diethyl-, trans- — 4I1-5 5- '- 29,20-29,40 29,60 29,80 m/z. 55.00 30.59%

5000 I -27- 84 J_ J 112 I '' ' ‘ I ' ' '' I ' ''' I ‘ .r' pl rn I I ... I I , rr I T . r TlZZ-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29,40 29.60 29.80

LB.D NP103001.M Mon Nov 05 08:56:56 2001 Page 5

NYC-WTC_000089288

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NYC-WTC_000089288Source: NYC Law Department, mirrored locally

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