GC/MS analysis results for sample AD23271, Oct 15 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT12 01\23271.D Vial: 19 Acq On : 12 Oct 2001 7:43 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Tetracosane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 31.74 6.06 ug/1 657500 Chrysene-dl2 33.12 Hit# Of 5 Tentative ID MW MolForm CAS# Qual Tetracosane 338 C24H50 000646-31-1 99 2 Octadecane 254 C18H38 000593-45-3 91 3 Docosane, 9-butyl- 366 C26H54 055282-14-9 91 4 Heneicosane 296 C21H44 000629-94-7 91 ‘Abundance Scan 2908 (31.735 min); 23271 ,D (-) m/z 57.00 100.00% 57

5000 85 4

Tife-> Abundance 40 MIUx 60 -T-fTTT''rp-i4nY*'TTTp-rT-ryrrrTYrT^^ 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 #73543; Tetracosane 338 '' I “ '' I 31.40 31.60 31,80 32.00 m/z71.0070.87%

57

5000 85 M 31.40 31.60 31.80 32.00 m/z 43.05 69.69% 1 I 113 155 183 294 338 I''' '' I' ' I''' ■' I'''' I'''' I'''' I I " '' I P ' “I " " I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #71561; Octadecane

5000 57

85 M 31.40 31.60 31.80 32.00 m/z 85.05 49.47%

TT-p-r I.1.1T > ■ ■ 111 r. I.. 11.. *11.... I.... I H ■. I ■. I. I.. I.... 11. H I ■ I > 11.... I ■. I. I. I nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73939; Docosane, 9-butyl- I ' ' ‘ 57 31.40 31.60 31.80 32.00 m/z41.05 27.89%

5000 85

4’ '' I'' I ii X I’l’ 252 309 TT^TyrTTTyrTTTyrTTTYTTTT^^ 366 TT-p-r • ■ I ■ ■ I • I I ■n/z-> 4060 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 31.40 31.60 31.80 32.00

23271.D NP091101.M Mon Oct 15 09:38:01 2001 Page 11

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