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GC/MS analysis results for sample AD23271, Oct 15 2001

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Laboratory report documenting GC/MS analysis of environmental sample AD23271 conducted on October 15, 2001.

NYC-WTC_000088372–000088401

Folder label: “GC/MS Scan 9/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23271.D Vial: 19 Acq On : 12 Oct 2001 7:43 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 1-Eicosanol Concentration Rank 17 R.T. EstConc Area Relative to ISTD R.T. 31.86 0.57 ug/1 62067 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qnal

1 1-Eicosanol 298 C20H42O 000629-96-9 93' 2 Acetic acid, octadecyl ester 312 C20H40O2i 000822-23-1 91- 3 1-Octadecanol 270 C18H38O 000112-92-5 74 4 1-Nonadecanol 284 C19H40O 001454-84-8 70 '\bundance Scan 2922 (31.864 min): 23271 .D (-) m/z 43.05 100.00% 43

81 gy 5000 111 I J 125 T _3t6g_3r80_JZ00_^,20_ 1 ,1, 207 m/z 83.05 57.85% Ti/z-> 40 60 80 100I 120 140 160 180 200 220 240 260 280 Abundance #72722:1-Eicosanol 57 83 69 97

5000 111 I ' n- 31.60 31.80 32.00 32.20 125 m/z 6^795 56.04% JUM 140I 160167 180 200 220 240 260 280 280 A I ' I Ti/z-> 40 60 80 100 120 Abundance #73048: Acetic acid, octadecyl ester 43 , ,.p-, 31.60 31.80 32.00 32.20 5000 m/z 97.05 53.38% 61 83 97 111 ..I: 139 224 252 ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72028:1-Octadecanol 57 8p _3t60_^t80_JZ00__3Z2g_ 69 97 m/z 55.00 51.02%

5000 111 I 125 I I I 140153 224 I' I'"'-'i“i' nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 31.60 31.80 32.00 32.20

23271.D NP091101.M Mon Oct 15 09:38:03 2001 Page 12

NYC-WTC_000088390

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NYC-WTC_000088390Source: NYC Law Department, mirrored locally

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