GC/MS calibration table for TCLP analysis, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File ; C:\HPCHEM\1\DATA\NOV0801\LBA.D Vial: 8 Acq On 8 Nov 2001 9:26 pm Operator: 209 GALOS Sample 10/19 lab blk Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 9-Eicosene, (E)- Concentration Rank 17 R.T. EstConc Area Relative to ISTD R.T. 31.81 0.54 ug/1 228178 Chrysene-dl2 33.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 9-Eicosene, (E)- 280 C20H40 074685-29-3 9 2 3-Eicosene, (E)- 280 C20H40 074685-33-9 9 3 1-Eicosanol 298 C20H42O 000629-96-9 93 4 1-Nonadecene 266 C19H38 018435-45-5 92 Abundance Scan 2916 (31.811 min): LBA.D (-) m/z 43 /05 100.00% 43

61 97 5000 111

r/z-> Abundance 1111}XXXXis^ 40 60 80 100 125

120 140 160 #39519: 9-Eicosene, (E)- 252 280 ■ j 1 ■ I I I ■ • ■ • I I I ■ ■ I ' > I I I I ■ I > (■ ■ 180 200 220 240 260 280 31.40 31.60 31.80 32.00 32.20 "m/z 83.05 64.69%

69 83

5000 97

111 MU/ 1 ‘ ' I ' 31 .y) 31.60 31.80 32.00 32.20

mZz-> Abundance LUI 40 60 80 , || 100 |[ 125 1^ 139................................................... 252 120 140 160 #39521:3-Eicosene. (E)- 180 200 220 240 260 280 280 m/z 4^1-05 61.10%

69 83 97 31,40 31.60 31.80 32.00 32.20 5000 m/z 97.05 60.76% 111 ft 125

m/z-> 40 60 80I LX 100I I I 139 120 140 160 180 200 220 240 252 260 280 280 Abundance if72722-. 1-Eicosanol I ' ' ' ‘ I ' ' ' ' I 83 3140_3lJB0_31J0_3Zg0_3Z^ 69 97 "m/z 55.00 58.45% 1 111 J ft 125

mZz-> T-rp-r 40 60 ' 80 100 120 133

140 160 167

180 200 220 240 260 280 280 XX ' 1 ' ' ' ' I 31.40 31.60 31.80 32.00 32.20

LBA.D NP103001.M Mon Nov 19 14:43:37 2001 Page 9

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