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GC/MS analysis results for sample AD23501, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23501 conducted on October 19, 2001.

NYC-WTC_000088853–000088879

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088874
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23501.D Vial: 9 Acq On : 16 Oct 2001 10:03 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Heneicosane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 35;50 3.04 ug/1 285673 Perylene-dl2 37.23 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 9T 2 Triacontane 422 C30H62 000638-68-6 91 3 Heptadecane, 9-octyl- 352 C25H52 007225-64-1 91 4 Heptacosane 380 C27H56 000593-49-7 91 Abundance Scan 3318 (35.498 min); 23501 .D (-) m/z 57.00 100.00% 57

5000 85 ,,.... i\..... . 35.20 35.40 35.60 35.80 ........................................ .............. . m/z 71.00 69.08% Tife-> 40 60 80 100120140160180 200220 240260280300320340 360380 400420 Abundance #42201: Heneicosane 57

85

35.20 35.40 35.60 35.80 m/ Z 43.00 63.88% |113 268 296 T I ‘' I " " I nfe-> 40 60 80 100120140160180 200220 240260280 300320340 360380400420 Abundance #55461: Triacontane 4 3- ' ' I ' ' 71 35.20 35.40 35.60 35.80 5000 m/z 85.05 46.72%

1 T ,1 1 239 267 379 422 pTTrj+rTTyrTVrpVrTyTrTTpTrrTpTTTpTTTpTTT^I^^ I H >> I I I I I pTi ■ I II <> I I I I I I II I I I I H

tVz-> 40 60 80 100120140160180 200220 240260280300320340 360380 400420 Abundance #49558: Heptadecane, 9-octyl- 57 -35.20 -35.40 - 35.60 35.80 ■m7T~^55~00 25.56%

5000 85

239 I 310 352 I I 11.|T, . .I,I.I I..I.f111.I..,.I I I pTTTpTTTY’TTrp-TTTy I ‘' I “ " I" " I Trrrrp-rrq- ■n/z-> 40 60 80 100120140160180 200220 240 260 280 300320340360 380 400 420 35.20 35.40 35.60 35.80

23501.D NP091101.M Thu Oct 18 10:21:52 2001 Page 15

NYC-WTC_000088874

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NYC-WTC_000088874Source: NYC Law Department, mirrored locally

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