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GC/MS analysis results for sample AD23501, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23501 conducted on October 19, 2001.

NYC-WTC_000088853–000088879

Folder label: “GC/MS Scan 9/27/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23501.D Vial: 9 Acq On : 16 Oct 2001 10:03 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table. 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 16 Hexatriacontane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 36.36 2.03 ug/1 190847 Perylene-dl2 37.23 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Eicosane, 7-hexyl- 366 C26H54 055333-99-8 91. 3 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 90 4 Pentacosane 352 C25H52 000629-99-2 87

JL Abundance Scan 3412 (36.361 min): 23501.D (-) m/z 57.00 10^700% 57 71 43 85 5000

I 1 99 113 36.00 36.20 36.40 36.60 , ■i n . J| ..... 72.34% ny2-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #74636: Hexatriacontane 43 57

71 5000 85 36.00 36.20 36.40 36.60 “mTz 4^700 627783% , | , '’J,^^169183197211 ................ ■nfe-> ^bundance 40

-43-57- 60 80 100 120 140 160 180 200 220 240 260 280 300 320 #50999: Eicosane, 7-hexyl- - ■-L- 71 36.00 36.20 36.40 36.60 5000 85 Wz 85.05 5^717%

I I, ll _ 169182197 I .... I f... 11111 11111 111.1111' 111111 1-11 .1 .1.... 1.1 I 281 310 TTTTJ n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #42196: Heptadecane, 2,6,10,15-tetramethyl- __ 57 36.00 36.20 -36.40-36;60------- __ ^71 m/z 55.00- 23.90%

5000 85

' I' I ' I, 'I ' q ■' T111 'i I. f. I. 183 211 111111 ’i 11,111 -1, 111.., 268 296 I' •' ’j 11. 11 ................................. ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 36.00 36.20 36.40 36.60

23501.D NP091I01.M Thu Oct 18 10:21:54 2001 Page 16

NYC-WTC_000088875

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NYC-WTC_000088875Source: NYC Law Department, mirrored locally

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