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GC/MS calibration table for TCLP analysis, Oct 2001

Machine-extracted title · confidence 95%

Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.

NYC-WTC_000086768–000086785

Folder label: “508 Scan

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0101\LBA.D Vial: 2 Acq On : 1 Oct 2001 2:41 pm Operator: 209 GALOS Sample : 9/14 Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Hexatriacontane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 36.40 0.59 ug/1 120164 Perylene-dl2 37.29 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Pentacosane 352 C25H52 000629-99-2 91 3 Tetratetracontane 619 C44H90 007098-22-8 91 4 Tetracosane 338 C24H50 000646-31-1 91 Abundance Scan 3416 (36.398 min): LBA.D (-) m/z 57.00 100.00% 57

5000 85

36.00 36.20 36.40 36.60 36.80 m/z 71.00 66731% TiZz-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #74636: Hexatriacontane 57

5000 85 T T T T 36.00 36,20 36.40 36.60 36.80

■n/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #73718: Pentacosane 43

36.00 36.20 36.40 36.60 36.80 71 Toy m/z 85.05 48.12%

______ 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #61068: Tetratetracontane 5(7 36.00 36.20 36.40 36.60 36.80 m/z55.0020.36% 5000 85

379407 590618 ■n/z-> 50 100 150 200 250 300 350 400 450 500 550 600 36.00 36.20 36.40 36.60 36.80

LBA.D NP091101.M Tue Oct 02 12:02:58 2001 Page 11

NYC-WTC_000086784

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NYC-WTC_000086784Source: NYC Law Department, mirrored locally

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