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GC/MS calibration table for TCLP analytes, October 2001

Machine-extracted title · confidence 90%

Calibration data table for TCLP analysis including retention times and response factors for various compounds.

NYC-WTC_000086981–000087006

Folder label: “508 Scan 9/17/01 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0101\LBD.D Vial: 4 Acq On : 1 Oct 2001 4:39 pm Operator:. 2 09 GALOS Sample : 9/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ***************************************■)(***•**************************

Peak Number 17 Hexatriacontane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 36.39 1.51 ug/1 221171 Perylene-dl2 37.28 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Dotriacontane 451 C32H66 000544-85-4 91 3 Tetracosane 338 C24H50 000646-31-1 90 4 Octadecane 254 C18H38 000593-45-3 90 Abundance Scan 3415 (36.393 min): LBD.D (-) m/z 56795 100.00% 5/ A 85 5000 A 3a00_36J0_J640_ja60_36^ 239 267..................... m/z 71.05 70.38% ■n/z-> Abundance 50

5|7 100 150 200 250 #74636: Hexatriacontane 300 350 400 450 ft 5000 85 I 36.00 36.20 36.40 36.60 36.80 Wz 43.05 65.24% 8 H/P.. 169 197 ' ' I I ttZz-> 50 100 150 200 250 300 350 400 450 Abundance #74491: Dotriacontane 57 T-p-r-r-r-p-r 36.00 36.20 36.40 36.60 36,80 5000 85 51.90%

I 196 281 422 450 ■nlz~> 50 100 150 200 250 300 350 400 450 Abundance #73543: Tetracosane 7 36.00 36.20 36.40 36.60 36.80 mTz 55700 24.32%

5000 85

y.A................ n/z-> 50 100 150 200 250 300 350 400 450 36.00 36.20 36.40 36.60 36.80

LBD.D NP091101.M Tue Oct 02 12:29:11 2001 Page 17

NYC-WTC_000087003

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NYC-WTC_000087003Source: NYC Law Department, mirrored locally

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