Calibration data table for TCLP analysis including retention times and response factors for various compounds.
NYC-WTC_000086981–000087006Folder label: “508 Scan 9/17/01 9/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0101\LBD. D Vial: 4 Acq On 1 Oct 2001 4:39 pm Operator: 209 GALOS Sample 9/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS7 5K.L ********************************************** * * ********************* Peak Number 18 Docosane Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T. 38.41 0.51 ug/1 74233 Perylene-dl2 37.28 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Docosane 310 C22H46 000629-97-0 90 2 Heptacosane 380 C27H56 000593-49-7 90 3 Tetratriacontane 479 C34H70 014167-59-0 87 4 Heneicosane 296 C21H44 000629-94-7 87 Abundance Scan 3635 (38.412 min): LBD.D (-) m/z 57700 100.00% 57
85 5000
207 38.00 38.20 38.40 38.60 38.80 I 281 "m/z 71.00 65793% nfe-> 40 60 80 100120140 160180 200 220 240 260 280 300 320 340 360 380 400 Abundance #44318: Docosane 57
85 5000 38.00 38.20 38.40 38.60 38.80 ■m/z 4^705 60.48% 266 310 I . 1 r| T1 r I I it Ti I 1) . 1 I 1 1 r I P / I . I I"' 11." 1111" I ■." I I"'H " "I"'' I" ''i I' I Tl/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 Abundance #52248: Heptacosane 57
38.00 38.20 38.40 38.60 38.80 5000 85 Tn/z 85705 53.01%
.. .1. .II. .ll,. jL .1 .'‘tv.281 324 380 ‘' I "' 7TYlT7TTTTYrT*r|-rtTT-]VrrVp-hTjTTTTjT-rTTjrrTTpT-rrjTTTTTTTTT^^ n/z-> 40 60 80 100120 140 160180 200 220 240 260 280 300 320 340 360 380 400 Abundance #58265: Tetratriacontane 7 38.00 38.20 38.40 38.60 38.80 “Wz ST/OO 21.32%
5000 85
A 367410 311 " I"' "'' I" " I''" I' " I I' " ' I " " I " '' I' " ' I I " ' ' T' 11' I " 11 p " ' I -n/z-> 40 60 80 100 120140 160 180 200 220 240 260 280 300 320 340 360 380 400 38.00 38.20 38.40 38.60 38.80
LBD.D NP091101.M Tue Oct 02 12:29:15 2001 Page 18
NYC-WTC_000087004
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NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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Laboratory results for sample AD22542 indicating other unknown compounds detected via GC/MS on September 27, 2001.
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Laboratory results for sample AD22544 indicating other unknown compounds detected via GC/MS on September 27, 2001.
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