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Document / 28 pages

GC/MS calibration table for TCLP analysis, Nov 2001

Machine-extracted title · confidence 100%

Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.

NYC-WTC_000069154–000069181

Folder label: “GCMS Scan X 10/19/01 An 11/8/01

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Scanned page image, NYC-WTC_000069163
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\1\DATA\NOV0801\LBA.D Vial: 8 Acq On : 8 Nov 2001 9:26 pm Operator: 209 GALOS Sample : 10/19 lab blk Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Docosane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 29.56 1.99 ug/1 838052 Chrysene-dl2 33.07 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Docosane 310 C22H46 000629-97-0( 2 Octadecane 254 C18H38 000593-45-3^1 3 Hexatriacontane 507 C36H74 000630-06-8 91 4 Heptadecane 240 C17H36 000629-78-7 91 Abundance Scan 2671 (29.562 min): LBA.D (-) m/z 57.00 100.00% 43 71 I 85 5000

I A 113 29.20 29.40 29.60 29.80 ||'l|. ,1*. /.A m/z 71.05 70.66% Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44318: Docosane 57 71 85 5000 29J0^402a60 29J0 99 m/z43.0569.72% I 113127141155.123 hl nl I I I ( 266 310 ......... 'I ' ' I ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I I ' ' ' ' I I ' ' ' ' I ' ' ' ' I ' ' I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #71560: Octadecane 43 5|7

71 29.20 29.40 29.60 29.80 U A, 5000 85 m/z8570050.87%

113 „| ,| 127141 169183197210 254 ' I ' ' I ' I ' ' ' ‘ ] ' ' ' ' [ ' ‘ ' I ' ' ' I ' ' ' ' I ' ' * ’ I ' ' ''' I mfe-> Abundance 40

43 57 60 80 100 120 140 160 180 200 220 240 260 280 300 #74636: Hexatriacontane ....... Ra...... 29.20 29.40 29.60 29.80 m/z 41.00 30717%

5000 71 85 I

■n/z-> 40 u 155169183197211 I ' ' '' I'''' I'''' r ''' I'' '' I'''' I'' '' I'''' r ''' r ''' I' '' ' I'''' I' ‘ 60 80 100 120 140 160 180 200 220 240 260 280 300 ' I .............. 29.20 29.40 29.60 29.80

LBA.D NP103001.M Mon Nov 19 14:43:26 2001 Page 4

NYC-WTC_000069163

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NYC-WTC_000069163Source: NYC Law Department, mirrored locally

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