GC/MS calibration table for TCLP analysis, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0801\LBA.D Vial: 8 Acq On : 8 Nov 2001 9:26 pm Operator: 209 GALOS Sample : 10/19 lab blk Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1-Hexene, 2-methyl- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 29.45 6.80 ug/1 2864900 Chrysene-dl2 33.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Hexene,>2r-methyl- 98 C7H14 006094-02-6 27 2 Cyclobut^^e, 1, l-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 3 Butyl iiexadecanoate 312 C2 0H40O2i 000000-00-0 25 4 Qxi^e, 2,3-bis (1-methylethyl)-, t 128 C8H16O 054644-32-5 23 Abundance" Scan 2659 (29 452 min): LBA.D (-) Fm/z 55795 100.00% 5|B

5000 41 73 239 257 .. L __292g^^40_2a60_ja8g_ p-rr-TT I I I . I I r. I I 1 I I I |-1 . I -I I . I I- r I I I 'I I I 1'' I I I 'p I r I I I •! I 11' I « Wz 57700 47.27% ■nfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #1354:1-Hexene, 2-methyl- sb

41 5000 29.20 29.40 29.60 29.80 27 70 m/z 43.05 37.46%

TiZz-> 20 40 'H

60 L 98 ' I 1 I I I « I I

80 I'' ■' 111' 1111111' 11' I''' ■ I 100 120 140 160 180 200 220 240 260 280 300 I'''' I' I Abundance #21985: Cyclobutane, 1,1-diinethyl-2-octyl- 53 I 29.20 29.40 29.60 29.80 5000 m/z 41.05 36.52%

27 70 I I, L ^111125140 168 196 I. . I T. . 1''| . , 1 , I , , . , I , , , I I . I . I'''' I I'''' I'''' I r ■nfz-> Abundance 20 40

53 60 80 100 120 140 160 180 200 220 240 260 280 300 #44549: Butyl hexadecanoate , La A I'''' I'''' I __2a20_^4g_ja60_2a80__ m/z 55.00 29.08% 258 I 240 312 , 129

J...II............ .. /lAA.,.. nfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

LBA.D NP103001.M Mon Nov 19 14:43:24 2001 Page 3

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