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GC/MS calibration table for TCLP analysis, Nov 2001

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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.

NYC-WTC_000069154–000069181

Folder label: “GCMS Scan X 10/19/01 An 11/8/01

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Scanned page image, NYC-WTC_000069161
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\1\DATA\NOV0801\LBA.D Vial: 8 Acq On : 8 Nov 2001 9:26 pm Operator: 209 GALOS Sample : 10/19 lab blk Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.56 ug/1 187107 1,4-Dichlorobenzene-d4 11.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichlpe^^benzene-d4 003855-82-1 58 150 C6C12D4 2 Benzene^sj 2,3,4-d4-, 5,6-dichloro- 002199-69-1 12 150 C6C12D4 3 IH-PyrXolo[2,3-b]pyridine-2,6-dione 152 C7H8N2O2 017384-56-4 9 4 Vanillin 152 C8H8O3 000121-33-5 9 Abundance Scan 711 (11.568 min): LBA.D (-) m/z 149.90 100.00% 1$0

552 115 78 52 1120 11.40 11,60 11.80

TT^-> 20 UiwUs Ui 30 40 50 60 70 80 90 Ji 4.^ m/z 151.90 . 59.87% 100 110 120 130 140 150 160 Abundance #9593; 1.4-Dichlorobenzene-d4 1!i0

5000 115 ■p"

78 11 20 11.40 11,60 11.80 52 m/z 114.90 35.05% 35 ' I'''' I' I' ''' I 44^ Ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2.3,4-d4-, 5,6-dichloro- 1!i0

115 11.20 11.40 11.60 11.80 5000 52 78 m/z78.05 19.65%

87

20 30 35 I 40 50 60 70 I ' I'''' I' 80 90 A 100 110 120 130 140 150 160 Abundance i#10125:1H-Pyrrolo[2,3-b]pyridine-2,6-dione, 3.3a,4,5-tetra 152 11 20 11.40 11.60 11.80 109 m/z 52700 14.29% 53 552 80 27 67 I 37 124 I '' ‘ ' I' ' ' ' I' '' ' I T ■nfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11,60 11.80

LBA.D NP103001.M Mon Nov 19 14:43:21 2001 Page 2

NYC-WTC_000069161

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NYC-WTC_000069161Source: NYC Law Department, mirrored locally

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