GC/MS calibration table for TCLP analysis, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C;\HPCHEM\1\DATA\NOV0801\LBA.D Vial: 8 Acq On : 8 Nov 2001 9:26 pm Operator: 209 GALOS Sample : 10/19 lab blk Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 7.69 1.16 ug/1 385868 1,4-Dichlorobenzene-d4 11.72

Hit# of 5 T^tative ID MW MolForm CAS# Qual

1 2-PentanQiie, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 47 2 3-Hydi^jty-2-pentanone 102 C5H10O2 003142-66-3 9 3 Mo: [boline, 4-methyl­ 101 C5H11N0 000109-02-4 9 4 ACj one 58 C3H6O 000067-64-1 9 Sundance Scan 288 (7.685 min); LBA.D (-) m/z 42.95 100.00% 43

5000 59

101 7.40 7.60 7.80 8.00 jJl Tq-n+ . 71 83 208 m/z 59.05 48.70% . ............. .................. TTfe-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.40 7.60 7.80 8.00 m/z 100.95 237771% 27 I I 83 I I'l . ( j I k . I I H I . J

TTfe-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #1691: 3-Hydroxy-2-pentanone 3) 59 __________ J '' I'''' I'''' I'' 7.40 7.60 7.80 8.00 5000 m/z 58.05 18.03% 45 15 1 73 84 *|TTTrp¥rTyTTTTpT-rT]^ 102 I ""I r I Tlfe-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #1640: Morpholine, 4-methyl- 43 _7:4gL_7,6g_^,8o_aoo^_ m/z 41.00 8.47% 5000 101 15 71

Tife-> I 86 4^ 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 I ‘'“1“" I"" I 7.40 7.60 7.80 8.00

LBA.D NP103001.M Mon Nov 19 14:43:19 2001 Page 1

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