Calibration record for GC/MS instrument using TCLP method, listing standard compounds and response data from November 6, 2001.
NYC-WTC_000069030–000069039Folder label: “GCMS Scan X 10/18/01 An 11/6/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data Pile : C:\HPCHEM\1\DATA\NOV0601\LBA.D Vial: 9 Acq On ; 6 Nov 2001 8:36 pm Operator: 209 G71LOS Sample : lb 10/18 Inst S GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.68 4.80 ug/1 962189 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tent^ive ID MW MolForm CAS# Qual 1 2-Pentanone, >4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 40 2 Acetone 58 C3H6O 000067-64-1 9 3 3-HydroxY/2-pentanone 102 C5H10O2 003142-66-3 9 4 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 9 Abundance c Scan 287 (7.681 min): LBA,D (-) m/z 42.95 100.00% 4)3
59 5000 101 7.40 7.60 7.80 8.00 71 ........ 1,1......... m/z 59.05^52.04% TiZz-> 10 20 30 40 50 60 80 70 90 100 110 Abundance #64275:2-Pentanone, 4-hydroxy-4-methyl- 4b
5000 59 ' 7.46' 7.^' ‘7.^ ' 8.66 ‘ m/z 101.0^ 22.78% IS 31 101 I I I 83 ■n&-> ' io' ' ' '20' ' ' 30' '~r+ tH- "1 ' ' ' ' I ' ' ‘ ■ I ' * I ' 40 60 70 80 90 100 110 Abundance #62 : Acetone 4b
7.40 7.60 7.80 8,00 5000 m/z 58.0^^ 18.32% 58 27 i-T-n-. I ' ‘ ' I ' ' ■ ‘ I ■ ' ' • I ' ■ ' ' I ' ' ' ' I ‘ •nfe~> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1691:3-Hydroxy-2-pentanone 3H 5b ' '7.^' ‘7.66' ‘7.80' 's.oo'' m/z 41.05 7.82% 5000 45 15 1„ I, 66 84 102 I I • ■ ■ ■ I • ■ ■ • I ■ ■ • • I • • ■ ■ I 1 ■ • • 1 • ■ -, , —..
n '' • ’ I • ’ • I ’ ’ • • (• * ‘ ’ I' rJz-» 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00
LBA.D NP103001.M Fri Nov 16 11:58:10 2001 Page 2
NYC-WTC_000069037
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NYC-WTC_000068815
Calibration data sheet for GC/MS instrument listing standards like naphthalene-d8 used for testing on November 6, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068230
Technical data sheet listing calibration standards and response factors for various polycyclic aromatic hydrocarbons.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067940
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 31, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069271
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069349
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 8, 2001.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069577
Calibration table data for GCMS analysis dated November 16-21, 2001, listing standard compounds and response values.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031054
Log sheet detailing sample preparation metrics for Method 608 analysis of WTC samples conducted in December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000030923
Calibration data for GC/MS analysis using Method 508 and TCLP procedures dated November 30, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087447
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000069027
Record of a GCMS scan conducted at the World Trade Center site in mid-November 2001.
Filed in the same folder
NYC-WTC_000069028
Fragmented document from DEP Box 60 containing unreadable text and sample identifiers, dated November 2001.
Filed in the same folder
NYC-WTC_000069040
Laboratory report documenting GCMS analysis of sample AD24880 conducted on November 19, 2001, noting unknown compounds.
Filed in the same folder
NYC-WTC_000069051
Laboratory report documenting GCMS analysis of sample AD24881 conducted on November 19, 2001, noting unknown compounds.
Filed in the same folder
NYC-WTC_000069062
Laboratory report documenting GCMS analysis of sample AD24944 identifying unknown compounds on November 19, 2001.
Filed in the same folder