Calibration data sheet for GC/MS instrument listing standards like naphthalene-d8 used for testing on November 6, 2001.
NYC-WTC_000068815–000068824Folder label: “GCMS Scan X 10/17/01 An 11/6/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data Pile : C:\HPCHEM\1\DATA\NOV0501\LBA.D Vial: 15 Acq On : 6 Nov 2001 1:37 am Operator: 209 GALOS Sample : 10/17 lb Inst ; GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 7.70 0.64 ug/1 106009 1,4-Dichlorobenzene-d4 11.71
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-PentanoneX^-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 42 2 5-Hexen-^Xone 98 C6H10O 000109-49-9 9 3 Morphqi-ine, 4-methyl- 101 C5H11N0 000109-02-4 9 4 Acetic acid, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 9 Abundance Scan 289 (7.700 min): LBA.D (-) m7z 43.05 100.00% 4)3
59 ssa 101 -TVTV, , , I ■ , rTirn-r
Tife-> 10 20 30 11 40 + 50 60 70 'I '' ' ' I 80 83 ' I ' 90 4100 no m/z 7.40 7.60 7.80 8.00 59.05 52.01%
Abundance #64275:2-Pentanone, 4-hydroxy-4-methyl- 4)3
5000 59 7.40 7.60 7.80 8.00 m/z 101.05 20.24% 15 31 101 ......... | I I 83 ‘ I ' ' ' ' I ’ T-pr-r-t ' I ' ■ ‘ ' I ' ' ‘ ■ I ' ' ' ' I ' nfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63205:5-Hexen-2-one 4)3 ’...................................................... ' ’ I ’ ' ’ * I ' * ' ' I * ' ’ ' I * ’ ‘ 7.40 7.60 7.80 8.00 5000 m/z 58.05 17.83%
55 15 27 I I 50 . I S3 98 Tife-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640: Morphottne, 4-methyl- 4)3 7.40 7.60 7.80 8.00 in/z 41.05 7.94%
5000 101 71 I 7, 1 ■ ■ ' ■ I • ■ 1 • I 56 '7.40 7.M' 7.80 8.66' TlZZ-> 10 20 30 40 50 60 70 80 90 100 110
LBA.D NP103001.M Tue Nov 13 12:15:22 2001 Page 2
NYC-WTC_000068822
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NYC-WTC_000069030
Calibration record for GC/MS instrument using TCLP method, listing standard compounds and response data from November 6, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068230
Technical data sheet listing calibration standards and response factors for various polycyclic aromatic hydrocarbons.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067940
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 31, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069271
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069577
Calibration table data for GCMS analysis dated November 16-21, 2001, listing standard compounds and response values.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069349
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 8, 2001.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000070089
DEP laboratory report documenting GC/MS results for sample AD25830 analyzed on December 6, 2001.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031054
Log sheet detailing sample preparation metrics for Method 608 analysis of WTC samples conducted in December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087447
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000068811
Record of a GCMS scan conducted at the World Trade Center site in mid-November 2001.
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NYC-WTC_000068812
Document page containing identification codes for GCMS scans conducted in November 2001 within DEP Box 60.
Filed in the same folder
NYC-WTC_000068825
Laboratory report documenting GCMS analysis of sample AD24697 with detection of unknown compounds on November 19, 2001.
Filed in the same folder
NYC-WTC_000068838
Laboratory report documenting GCMS analysis of sample AD24696 identifying unknown compounds on November 19, 2001.
Filed in the same folder
NYC-WTC_000068853
Laboratory report documenting GCMS analysis of sample AD24698 identifying unknown compounds on November 19, 2001.
Filed in the same folder