Calibration data sheet for GC/MS instrument listing standards like naphthalene-d8 used for testing on November 6, 2001.
NYC-WTC_000068815–000068824Folder label: “GCMS Scan X 10/17/01 An 11/6/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File s C:\HPCHEM\1\DATA\NOV0501\LBA.D Vial: 15 Acq On : 6 Nov 2001 1:37 am Operator: 209 GALOS San^jle : 10/17 lb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 6.41 0.68 ug/1 113298 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolFoirm CAS# Qual 1 2-Hexanone 100 C6H12O 000591-78-6 86 2 2-Hexanq; , 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 3 Oxira; ; 2-methyl-2-(l-methylethyl) 100 C6H12O 072221-03-5 64 4 Mepif1 Isobutyl Ketone____________ 100 C6H12O 000108-10-1 53 Abundance Scan 149 (6.415 min): LBA.D (-) m/z 42.95 100.00% 43
58 5000
-J-1 -F T -T J : I . . J . . . . I . . . T I . I 6.00 6.20 6.40 6.60 6.80 51 I, 71 T T ' 1 ’''' 1 ‘''' I'''' I'''' I' ‘‘ I'''' I' ‘ ‘ ‘ I' m/z 58.05 57.05% Tife-> » " ab'' 40 50 60 70 80 90 100 110 120 130 140 Abundance #63384:2-Hexanone 43
5000 58 I ' ' ' ' 1 ' ' ' I'''' I' ‘' r'' 6.00 6.20 6.40 6.60 6.80 29 “m/z 4170^ 16774% 71> 85 100 I, I I
nfe-> 20 30 40 so’' ro 70 ' iro go' -ioo iio i^M "uo Abundance #11968:2-Hexanone. 4-hydroxy-3-propyl- 43 58 6.00 6.20 6.40 6.60 6.80 5000 29 "m/z 57760 16.35%
T)Zz-> 20 1'1'' ‘ ‘ I • • • • 11 30 40 ,1, ' I ‘' I ‘ 7,1 85 ,.|l|.,, 11, ,1,1),,,
50 60 70M 90 100 110 120 100 I 11 11 I 11 I 11 11
130 140
Abundance #1530: Oxirane, 2-mrthyl-2-(1-m^ylethyl)- 413 6.00 6.20 6.40 6.60 6.80 58 m/z 100.05 10.69% 5000 71 30 85 100 \A^V\ A / I'''' I' T-p-rV ufe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.00 ' ' 6.^ ' 6.40 6.60 6.80
LBA.D NP103001.M Tue Nov 13 12:15:11 2001 Page 1
NYC-WTC_000068821
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NYC-WTC_000069030
Calibration record for GC/MS instrument using TCLP method, listing standard compounds and response data from November 6, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068230
Technical data sheet listing calibration standards and response factors for various polycyclic aromatic hydrocarbons.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067940
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 31, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069271
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069577
Calibration table data for GCMS analysis dated November 16-21, 2001, listing standard compounds and response values.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069349
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 8, 2001.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000070089
DEP laboratory report documenting GC/MS results for sample AD25830 analyzed on December 6, 2001.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031054
Log sheet detailing sample preparation metrics for Method 608 analysis of WTC samples conducted in December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087447
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000068811
Record of a GCMS scan conducted at the World Trade Center site in mid-November 2001.
Filed in the same folder
NYC-WTC_000068812
Document page containing identification codes for GCMS scans conducted in November 2001 within DEP Box 60.
Filed in the same folder
NYC-WTC_000068825
Laboratory report documenting GCMS analysis of sample AD24697 with detection of unknown compounds on November 19, 2001.
Filed in the same folder
NYC-WTC_000068838
Laboratory report documenting GCMS analysis of sample AD24696 identifying unknown compounds on November 19, 2001.
Filed in the same folder
NYC-WTC_000068853
Laboratory report documenting GCMS analysis of sample AD24698 identifying unknown compounds on November 19, 2001.
Filed in the same folder