GCMS calibration table, sample AD23914, Oct 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\LBA.D Vial: 11 Acq On : 17 Oct 2001 11:05 pm Operator: 209 GALOS Sample : lab blk 10/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.49 0.88 ug/1 87682 l,4-Dichlorobenzene-d4 11.76 Hit# Of 5 ative ID MW MolForm CAS# Qual 1 2-Hexane^ 100 C6H12O 000591-78-6 91 2 2-Hex^one, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 3 Oxir.ane, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 64 4 2-^^xanone, 4-hydroxy-5-methyl-3-pr 172 C10H20O2: 061141-74-0 59 ^bundq^e Scan 157 (6.485 min): LBA.D (-) m/z 42795 100.00% 43

58 5000

71 85 100 6.20 6.40 6.60 6.80 I, I . . . . I , . . ,l|l| Ji].,,,. J,,,.,,. .. ■m/z 58.05 57792% TiZz-> 20 30 40 50 60 70 TO 90 100 110 120 130 140 Abundance #1556:2-Hexanone 43

58 __ , 5000 6.20 6.40 6.60 6.80 “m/z 41.05 15.83% 27 71 85 100 ■ I ‘' I ‘ ‘ ‘SI' I I ■ I •' ’ • I' ’ ' ’ I ■ ■ ■ ' I ■ ■ ■ ■ 1 • ■ I''' I ■ ■' ‘ I ■ ‘ ‘ ■ I'''' I • n&-> 20 30 40 50 60 70 TO 90 100 110 120 130 140 Abundance #11968:2-Hexanone, 4-hydroxy^propyI- 43

58 T 6.20 6.40 6.60 6.80 5000 29 m/z 57.00 14.69%

nfe-> 20 ' I'''' 11'' ■ I ■ 30 40 50 ,1, 60 7O8O 90 100 110 1M13O ................. .. 140 140 Abundance #1530: Oxirane, 2-methyl-2-(1-methyIethyl)- 4t3 ' ' 6j6 ' ' 6.TO ' ‘ 6.TO' ‘ 6.80' ' ' 58 m/z 100.05 9794%

IL 5000 71

30 85 100 ■ I •' ■ • I ■ • ■ ■ 11 nZz-> 20 30 40 50 eb''' tG' '' TO " 100110120130140 6.40 6.60 6.80

LBA.D NP101901.M Tue Oct 23 12:53:56 2001 Page 2

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