GCMS calibration table, sample AD23914, Oct 2001

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Library Search Confound Report

Data File : C:\HPCHEM\1\DATA\OCT1701\LBA.D Vial: 11 Acq On : 17 Oct 2001 11:05 pm Operator: 209 GALOS Sample : lab blk 10/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPC3IEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L Peak Number 1 3-Hexanone Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.38 0.42 ug/1 41552 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 tentative ID MW MolForm CAS# Qual 1 3-HexanMe 100 C6H12O 000589-38-8 83 2 2,4-Pentanedione 100 C5H8O2 000123-54-6 38 3 Hexaije, 3,3,4- trimethyl - 128 C9H20 016747-31-2 36 4 But^e, 2,2-dimethyl- 86 C6H14 000075-83-2 36 Abundar^ ■ Scan 146 (6.384 min): LBA.D (-) m/z 43.05 100.00% 40 57 71 5000 100

6.00 6.20 6.40 6.60 6.80 1-kpTTTpTTTrfn +p.Tpm^ m/z 56.95 94.58% TiZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #63358:3-Hexanone 43 57

5000 71 6.00 6,20 6.40 6.60 6.80 100 m/z 71700 69.18%

Tife-> 4bundanc8

5000 ++prTTpTTp 20253035404550556065 70 75 808590^ 100105110115120

43 #63324:2,4-Pentanedione p-m-fr 85

85 100 u 6.00 6,20 m/z 100.05 6.40 6.60 6.80 36.21%

27 .58 72 P?§^ ip<,.p,,<|,.i,p.,.p,,,pli,p,,,i i..,p<,ip,i,p,>,i TiZz-> 202S303540455055a)65 70 75 80 85 90 95 100105110115120 Abundance #5135: Hexane, 3,3,4-trimethyI- 40 57 71 6.6o 6.^ 6.40 6.60 6.80 "inTz 40.95 35.62%

5000

27 99 npTrrp4TTpTTpTTTpTWTpTTpTTH I I I , | i i . . | , i I I I , . | 113 . p . . . । i . . . । . . . . |. II | . i.i | iii . ।. I . ।. . . , । .

■nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 6.00 6.20 6.40 6.60 6.80

LBA.D NP101901.M Tue Oct 23 12:53:54 2001 Page 1

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