Calibration record for GC/MS instrument using TCLP method, listing standard compounds and response data from November 6, 2001.
NYC-WTC_000069030–000069039Folder label: “GCMS Scan X 10/18/01 An 11/6/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File s C:\HPCHEM\1\DATA\NOV0601\LBA.D Vial: 9 Acq On : 6 Nov 2001 8:36 pm Operator: 209 GALOS Sample : lb 10/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.42 0.68 ug/1 136144 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 2-Hexanoi^ 100 C6H12O 000591-78-6 91 2 2-Hexanone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 83 3 Oxirai^ 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 72 4 Methyl Isobutyl Ketone_________ 100 C6H12O 000108-10-1 58 Abundance Sean 150 (6.424 min): LBA.D (-) m/z 43.05 100.00% 43
58 500)
UI I, 11|' 6.00' rm' 6.^' 6.^ aro ■ra/z 58.00 61.30% TiZz-> 20 30 40 50 TO 70 80 90 100 110 12) 130 140 Abundance #1556:2-Hexanone 43
58 5000 6.00 6.20 6.40 6.60 6.80 "mTz 57700 17.81% 27 I ' I'' ' ' 1 ' Tife-> 20 30 40 50 60 ‘70 ' ‘ 'sb' ' '90 ‘'iro'' 116' ‘ w ' w‘ TSo Abundance #11968:2-Hexanone, 4-hydroxy-3-propyl- 43
58 .rmI^TSI^^rSI^rSZrotL. 5000 29 "mTz 41.05 16.18%
' I ‘ ' ‘ ‘ I ' • • ■ I I ,1 140 infe-> Abundance 20 30 40 ' 1 ‘ ‘ ' 50 60 '70 ' 80' 90' ' 166' ‘ 116'' w 'w TSo #1530: Oxirane, 2-methyl-2-{1-methylethyI)- 4i3 6.66' 'sjao' 6.40' 6,^ 58 m/z 100.05 12.94% 5000 71
30 85 100 '' I ■ ■ " I " " 11' • I ■ 1 1 . 1 1 I 1 I ■ 1 1 . -1 "i-'i I I I . I ,-1 . . I . r- infe-> 20 30 40 50 60 70 80 90 ioo iio 'w' 'w' '146 6.00 6.20 6.40 6.60 ‘ 6.80 - --
LBA.D NP103001.M Fri Nov 16 11:58:08 2001 Page 1
NYC-WTC_000069036
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NYC-WTC_000068815
Calibration data sheet for GC/MS instrument listing standards like naphthalene-d8 used for testing on November 6, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068230
Technical data sheet listing calibration standards and response factors for various polycyclic aromatic hydrocarbons.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067940
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 31, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069271
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069349
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 8, 2001.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069577
Calibration table data for GCMS analysis dated November 16-21, 2001, listing standard compounds and response values.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031054
Log sheet detailing sample preparation metrics for Method 608 analysis of WTC samples conducted in December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000030923
Calibration data for GC/MS analysis using Method 508 and TCLP procedures dated November 30, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087447
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000069027
Record of a GCMS scan conducted at the World Trade Center site in mid-November 2001.
Filed in the same folder
NYC-WTC_000069028
Fragmented document from DEP Box 60 containing unreadable text and sample identifiers, dated November 2001.
Filed in the same folder
NYC-WTC_000069040
Laboratory report documenting GCMS analysis of sample AD24880 conducted on November 19, 2001, noting unknown compounds.
Filed in the same folder
NYC-WTC_000069051
Laboratory report documenting GCMS analysis of sample AD24881 conducted on November 19, 2001, noting unknown compounds.
Filed in the same folder
NYC-WTC_000069062
Laboratory report documenting GCMS analysis of sample AD24944 identifying unknown compounds on November 19, 2001.
Filed in the same folder