Calibration record for GC/MS instrument using TCLP method, listing standard compounds and response data from November 6, 2001.
NYC-WTC_000069030–000069039Folder label: “GCMS Scan X 10/18/01 An 11/6/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Confound Report Data File : C:\HPCHEM\1\DATA\NOV0601\LBA.D Vial: 9 Acq On : 6 Nov 2001 8:36 pm Operator: 209 GALOS Sample : lb 10/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L A********************************'*******************'***************'** Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.55 ug/1 110932 1,4-Dichlorobenzene-d4 11.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorobez(zene-d4 150 C6C12D4 003855-82-1 42 2 Benzene-1,2^^4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 35 3 Acenaphthylene 152 C12H8 000208-96-8 10 4 Biphenyl^e 152 C12H8 000259-79-0 7 Abundance Z Scan 711 (11.574 min): LBA.D (-) m/z 149.90 .100.00% 1$0
5000 115 78 __ 52 I'' 11.20 11.40 11.60 11.80 12.00
TlZz-> 36. ' ‘ I ''' ' I 30 40 , I, . 62 111 I I /11 I I 50 60 UUSn I m/z 151.90 . 64.80% ' 1 ‘ ‘ ‘ 70 80 90 100 110 120 130 140 150 160 1
Abundance #9593:1,4-Dichlorobenzene-d4 1!0
5000- 115 T 78 1120 11.40 11.60 11.80 12.00 52 m/z 115.00 37.07% 35 1" • ’ 1 nfe-> " 40' 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1!i0
115 11.26' i'i!4b I'teo' '1'1!^ 12'oio 5000 52 78 m/z 78.05 . 19.31%
35 87 I 1 ‘ I ' ' ' ' I ' p ‘ ‘ • I ‘ 1 ’ ’'' I Ti^-> 30 40" ' 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #67015: Acenaphthylene 1!i2 1120 11.40 11.60 11.80 12.00 m/z 52.00 15.35%
5000-
63 7 1^ II 7^ nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00
LBA.D NP103001.M Fri Nov 16 11:58:12 2001 Page 3
NYC-WTC_000069038
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NYC-WTC_000068815
Calibration data sheet for GC/MS instrument listing standards like naphthalene-d8 used for testing on November 6, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068230
Technical data sheet listing calibration standards and response factors for various polycyclic aromatic hydrocarbons.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067940
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 31, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069271
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069349
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 8, 2001.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069577
Calibration table data for GCMS analysis dated November 16-21, 2001, listing standard compounds and response values.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031054
Log sheet detailing sample preparation metrics for Method 608 analysis of WTC samples conducted in December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000030923
Calibration data for GC/MS analysis using Method 508 and TCLP procedures dated November 30, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087447
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000069027
Record of a GCMS scan conducted at the World Trade Center site in mid-November 2001.
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NYC-WTC_000069028
Fragmented document from DEP Box 60 containing unreadable text and sample identifiers, dated November 2001.
Filed in the same folder
NYC-WTC_000069040
Laboratory report documenting GCMS analysis of sample AD24880 conducted on November 19, 2001, noting unknown compounds.
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NYC-WTC_000069051
Laboratory report documenting GCMS analysis of sample AD24881 conducted on November 19, 2001, noting unknown compounds.
Filed in the same folder
NYC-WTC_000069062
Laboratory report documenting GCMS analysis of sample AD24944 identifying unknown compounds on November 19, 2001.
Filed in the same folder