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GCMS analysis results, sample AD23905, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23905 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067522–000067534

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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NYC 9/11 Public Portal Document

Library Search Confound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23905.D Vial: 10 Acq On : 17 Oct 2001 10:07 pm Operator: 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.62 0.52 ug/1 50792 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlor^enzene-d4 150 C6C12D4 003855-82-1 64 2 Benzene-1^2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 38 3 Benzena^ne, 2-methyl-4-nitro- 152 C7H8N2O2; 000099-52-5 14 4 BenzajLdehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 abundancez Scan 717 (11.620 min): 23905.D (-) m/z 149.90 100.00% 1!i0

5000 115 52 78 K* ‘ * 1 ’ • 40 I 11,20 11.40 11.60 11.80 12.00

T)fe-> Tr-[ ■ ■ i-vl I 1 ■ I I I I ?i-|-r 30 40 50 60 UUJn 70 80 90 I 100 110 120 130 140 150 160 m/z 151.90 63.56% Abundance #9593:1.4-Dichlorobenzene-d4 liiO

5000 115 78 11.23 11.40 11.60 11.80 12.00 52 m/z 115.00 38.29%

nfe-> 30 35 40 50 60 70 80 90 100 110 120 130 140 150 160 3Lt ■i... M)undance #9592: Benzene-1.2.3,4-<i4-, 5.6-dichloro- 1!0

115 11.20 11.40 11.60 11.80 12.00 5000 52 78 “m/z 78.05 19.12%

35 87 ft I I 4^ ‘ I ' ' * ‘ I ‘ ‘ ‘ I ' • ■ I ■ nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10129: Benzenamine, 2-methyi-4-nitro- ......... ............. 77 106 15 a 11.a3 11.40 11.60 11.80 12.00 “mTz 52.00 17.36%

5000 51 94

' I'''' I'''' I T TlZ2-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

23905.D NP101901.M Tue Oct 23 12:51:56 2001 Page 4

NYC-WTC_000067533

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NYC-WTC_000067533Source: NYC Law Department, mirrored locally

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