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GCMS analysis results for sample AD24289, Nov 5 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24289 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068145–000068157

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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Scanned page image, NYC-WTC_000068155
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NYC 9/11 Public Portal Document

Library Search Confound Report Data File : C:\HPCHEM\1\DATA\OCT3101\24288.D Vial: 9 Acq On : 31 Oct 2001 11:55 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.51 ug/1 65917 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 ntative ID MW MolForm CAS# Qual 1 1,4-Dichl^obenzene-d4 150 C6C12D4 003855-82-1 47 2 Benzene-^2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 36 3 ((3-Etho^henyl)-1-methanol 152 C9H12O2 000000-00-0 10 4 Acenaphthylene _______________________ 152 C12H8 000208-96-8 9 Abundance Scan 711 (11,573 min): 24288,0 (-) m/z 149.90 100.00% 1!i0

5000 115 78 52 11.20 11.40 11,60 11.80 12.00

nZz-> 30 39 40 50 60 70 87 ''' 1 ■ 80 90 100 110 120 130 T JI 140 150 160 m/z 151.90 . 60.02% Abundance #9593:1,4-Dichiorobenzene-d4 1$0

5000 115 78 11.20 11.40 11.60 11,80 12.(X) 52 m/z 114.90 38.87% 35 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2.3,4-64-, 5,6-dichloro- 1!i0

115 11.20 11.40 11.60 11.80 12.00 5000 52 78 m/z 78.05 . 22.72%

87

nZz-> 30 35 1 _ _________________ I ' I ‘ ‘ 40 ' I 50 ’'' I'' ‘ ‘ I ‘' 60 70 80 I' ‘ ‘' I' 90 100 110 A 120 130 140 150 160 <U>undance #10217: ((3-Ethoxyphenyl)-1-methanol 1!i2 I’l^ao' 'ii‘4o 'i?eD 'I'i'so' 'izoo 95 m/z 52.10 , 15.01% 77 123 5000 106

67 89 ' 1 ' ' ‘ ' 1 ‘ ‘ ‘ ' I ' ‘ ■nfe-> MZZ^ZZ^M TOZ roZSZ 100110 l£130 140 1M1OT 11.20 11.40 11.60 11.80 12.00

24288.D NP103001.M Fri Nov 02 12:00:48 2001 Page 3

NYC-WTC_000068155

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NYC-WTC_000068155Source: NYC Law Department, mirrored locally

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