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GCMS analysis results, sample AD23904, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23904 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067508–000067521

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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Scanned page image, NYC-WTC_000067520
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NYC 9/11 Public Portal Document

% Library Search Confound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23904.D Vial: 9 Acq On : 17 Oct 2001 9:08 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.62 0.54 ug/1 57492 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tei>tative ID MW MolForm CAS# Qual 1 1,4-DichL0cfbbenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzen^Xl,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 35 3 Benza^ehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 4 Biphenylene 152 C12H8 000259-79-0 9 e Scan 717 (11.621 min): 23904.D (-) m/z 149.90 100.00% 1$0 fl

5000 115 78 ........ ............ 87 11.:y 11.40 11.60 11.80 12.00

nZz-> 30 40 50 60 70 ''' I' 80 90 ‘ ‘ I 100 110 120 130 140 150 160 4U- m/z 151.90 59.77% Abundance #9593:1,4-Dichlorobenzene-d4 1ii0

5000 115 -r-r-|-r-r 78 11.20 11.40 11.60 11.80 12.00 52 m/z 115.00 35.72% 35 ...... ‘ I Ti/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-. 5,6-dichloro- 1!i0 1 ' ' ' ' I ' ' 115 11.20 11.40 11.60 11.80 12.00 5000 52 78 "m7z 78.05 19.69%

87

TTfe-> 30 35 I 40 50 * 1' ’ * ’ I ’ 60 7080 I T I p t. 111 90 100 110 120 130 140 A I ’ ’ ' ’ I 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- I ' ' ' ' I ' ' ' ' I ' ' 1ii2 11.^ 11.40 11.60 11.80 12.00 “m/z 52.00 15.81% 53 106 A 5000 81

92 122 136 ....... T-p-r-n-p-r-r-r-j- • I ' ' * • I ' • • • I • T ' ' I ' Tlfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11,40 11,60 11.80 12.00

23904.D NP101901.M Tue Oct 23 12:50:56 2001 Page 5

NYC-WTC_000067520

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NYC-WTC_000067520Source: NYC Law Department, mirrored locally

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