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GCMS analysis results, sample AD23913, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23913 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067601–000067618

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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Scanned page image, NYC-WTC_000067617
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NYC 9/11 Public Portal Document

Library Search Confound Report Data File : C:\HPCHEM\1\DATA\OCT1801\23913.D Vial: 6 Acq On : 18 Oct 2001 9:05 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPC3IEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.63 0.54 ug/1 52909 1,4-Dichlorobenzene-d4 11.77 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorob/nzene-d4 150 C6C12D4 003855-82-1 87 2 Benzene-l,2,/,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 40 3 Acenaphthylauie 152 C12H8 000208-96-8 10 4 2-Methyl-6ynitroaniline____________ 152 C7H8N2O2 000570-24-1 10 Abundance / Scan 718 (11630 min): 23913.D (-) Tm/z 149.90 100.00% liO

5000 115 78 52 11.20 11.40 11.60 11.80 12.00 40 I 87 ■' I ■ ■' ■ I • I.. (11 (111 I ’' '' I 4 ra/z 151.90 . 59.78% nZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 *\bundance #9593; 1,4-Dichlorobenzene-<l4 1!i0

5000 115 I . ■ . . I i . |-r,

78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 , 35.95% 35 87 Tife-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 T-X- Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1!i0

115 11.^ 11.40 11.60 11,80 1200 5000 52 78 “mTz 78.05 20.61%

87

TiZz-> 30 35 I 40 50 ■ I'''' I ' 60 70 I ' I'''' I' T 80 90 100 110 120 130 A 140 150 160 Abundance #67015: Acenaphthylene It 2 11.20 11.40 U.K) 11.80 12.00 “Wz 52.00 14711% 5000

76 63 • ■ I • • ■ • I ■ • • ■ I • ■ • • 11 ■ 87 98 I ’' ■' I 126 l-T-rl-r- 11 Tife-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160

23913.D NP101901.M Tue Oct 23 14:34:39 2001 Page 3 NYC-WTC_000067617

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NYC-WTC_000067617Source: NYC Law Department, mirrored locally

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