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GCMS analysis results for sample AD24289, Nov 5 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24289 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068145–000068157

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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Scanned page image, NYC-WTC_000068154
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3101\24288.D Vial: 9 Acq On : 31 Oct 2001 11:55 pm Operator: 209 GALOS San^jle : gc/ras unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.70 0.90 ug/1 115822 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 2-PentanQzIe, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 39 2 4-Hydro^-3-hexanone 116 C6H12O2 004984-85-4 23 3 5-Hex^2-one 98 C6H10O 000109-49-9 9 4 Oxir^e, [ (1-methylethoxy)methyl] - 116 C6H12Q2 004016-14-2 9 Mwdance Sran 289 (7.699min): 24288.D (-) m/z 42.95 100.00% 40

59 5000 101 ' 7.^' 7,^ 8.ro •nfe-> 10 20 30 40 4Mb 50 60 ' I ■ ' ' ' I 70 80 . I I . . . I I . I 1 . I 1 I 1 I I 1 90 100 110 120 m/z 59.05 55.70% Abundance #3245; 2-Pentanotw, 4-hydroxy-4-methyl- 4)3

5000 59 7.40 7.60 7.80 8.00 m/z 100.95 30.06% 31 83 101 I,, I I I , I , , , , ,1,^1’ I , I , I 73 TiZz-> 10 20 30 40 50 60 70 80 90 100 110 120 ^bundanc8 #3241:4-Hydroxy-3-hexanone 50 ■ ■ I 'l I I . . I J. I I I ■ . ■ .

31 7.40 7.60 7.80 8.00 5000 m/z 58.05 16.48%

I 45 87 116 ' I ' ' ‘ ' 1 ■ ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' Tife-> 10 20 30 40 50 60 70 80 90 100110120 Abundance #63205:5-Hexen-2-one 43 ' 7.^ 7.^ 7.80 8.^' ' m/z 41.05 8.43% 5000

55 .1 83 98 ' I ■ ‘ ‘ I ' ' ■ ■ I ■ ‘ ■ 1 ' ‘ ■ 1 ' ' ■ ■ I ' ' ■ ■ I ' ‘ ' I ' I ‘ ' I 1 ' • • ' I ■ ' ‘ ■ I ' Tlfe-> 10 20 30 40 50 60 70 80 90 100 110 120 7.40 7.60 7.80 8.00

24288.D NP103001.M Fri Nov 02 12:00:46 2001 Page 2

NYC-WTC_000068154

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NYC-WTC_000068154Source: NYC Law Department, mirrored locally

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