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GCMS analysis results, sample AD23905, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23905 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067522–000067534

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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Scanned page image, NYC-WTC_000067532
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23905.D Vial: 10 Acq On : 17 Oct 2001 10:07 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.76 1.51 ug/1 147461 1,4-Dichlorobenzene-d4 11.77 Hit# Of 5 Tenifative ID MW MolForm CAS# Qual 1 2-Pentanorxe, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 40 2 S-Hexen^-^one 98 C6H10O 000109-49-9 9 3 Morphipline, 4-methyl- 101 C5H11N0 000109-02-4 9 4 3-Hyd:roxy-2-pentanone 102 C5H10O2 003142-66-3 9 ^bundancaf Scan 296 (7.755 min): 23905.D (-) m/z 43.00 100.00% 43

59 5000

101 7.40 TJTO 7.80 8.00

TiZz-> Ih XXr 207 I"''!' 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 ra/^ 59.05 50.63% Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl-

jL 'Its

5000 59 740 7.60 7.80 8.00 m/z 101.05 19.65% 27 I I 10 2030405060 70 8090 100110120130140150160170180190200210 \bundance #63205:5-Hexen-2-one 43 IJ11 1111111 7.40 7.60 7.80 8.00 5000 m/z 58.05 16.13% 55 83 98 pVrTfTTTtp Tife-> 10 2030405060 70 80901O01101201OT1401501OT170180190200210 Abundance #63448: Morpholine, 4-methyl- 43 7.40 TOT 7.80 8.00 m/^ 41.05 6.68% 5000

101

Tlfe-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 7.40 7.60 7.80 8.00

23905.D NP101901.M Tue Oct 23 12:51:54 2001 Page 3 NYC-WTC_000067532

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NYC-WTC_000067532Source: NYC Law Department, mirrored locally

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