GC/MS calibration table for TCLP analytes, October 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0101\LBD.D Vial: 4 Acq On 1 Oct 2001 4:39 pm Operator: 209 GALOS Sample 9/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Tetracosane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 31.77 2.70 ug/1 421315 Chrysene-dl2 33.16 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane 338 C24H50 000646-31-1 99 2 Octadecane 254 C18H38 000593-45-3 91 3 Heneicosane 296 C21H44 000629-94-7 91 4 Eicosane 282 C20H42 000112-95-8 87 Abundance Scan 2911 (31.766 min): LBD.D {-) m/z SYTOO 100.00%

71 43 85 5000

113 IL ' ' 1 ' ' 31.40 31.60 31.80 32.00 1 iJ iJ "I 155169183197211225239253267281 338 O-L I IT I I I" 11 q 11 f 11 rI 11J111A 11 r 111 "i I I r 111"k 111' 11 'I'l 1111111111-1111111 '' I'''' I'' m/z 71.10 70.76% Tl/Z~> ' 40 '' 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57

JI 71

5000 85 T 31 40 31.60 31.80 32.00 99 m/z 43705 64.32% \]3127 155169183197 338 294 I " 111' " ' I'' " I " " I " " I' " ' I " " I' " ' I ’ " ' I " " I' " ' I'' Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71561: Octadecane 57 43 71 31.40 31.60 31.80 32.00 85 5000 m/z 85.05 50.02%

224 'I I'111,, 1111.1,1 I ' ' * ' I ' I''' ‘ I'''' I I'''' I 1' " 'T 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ■n/z-> Abundance 40

5(7 #42201: Heneicosane __ A/q.,...,, 31.40 31.60 31.80 32.00 71 m/z 41.05 26.93% 85 5000

99 268 296 '' I'' I ’'' ' I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

LBD.D NP091101.M Tue Oct 02 12:28:49 2001 Page 12

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