Calibration data table for TCLP analysis including retention times and response factors for various compounds.
NYC-WTC_000086981–000087006Folder label: “508 Scan 9/17/01 9/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0101\LBD.D Vial: 4 Acq On : 1 Oct 2001 4:39 pm Operator: 209 GALOS Sample : 9/17 Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DAT7kBASE\NBS75K.L ********************************************************************* Peak Number 11 Butyl tetradecanoate (myristat Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T. 31.67 2.96 ug/1 461621 Chrysene-dl2 33.16 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Butyl tetradecanoate (myristate) 284 C18H36O2; 000000-00-0 80 2 Octadecanoic acid, 2-methylpropyl e 340 C22H44O2: 000646-13-9 46 3 Octadecanoic acid, butyl ester 340 C22H44O2; 000123-95-5 38 4 1-Hexene, 2-methyl- 98 C7H14 006094-02-6 27 Abundance Scan 2901 (31.674 min): LBD.D (-) m/z 56.00 100.00% 53
4 73 129
TiZz-> 40 IM 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 m/z 31.40 31.60 31.80 32.00 57700 51.01% Abundance #40186: Butyl tetradecanoate (myristate) 53
.................... 5000 229 31.40 31.60 31.80 32.00 , ” '29 211 m/z 41700 41734% 284 1 I''' ‘ I'''' I'''' r ''' I ' 11''' I ‘' I'''' I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 5(7
31.40 31.60 31.80 32.00 aiiiii; in/z 41.00 33777% 285 340
vL -n-p-r T-tT-^-r\'rrYT-rr-ry-rr'TTYri-rrYrT-r-rYt-ri--rTyrT-rYr-!-rr-f-T-^^ Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48208: Octadecanoic acid, butyl ester T 53 31.40 31.60 31.80 32.00 m/z -73.00 29.49%
5000 285 73 129 267 340 185 241 ' ' I ‘ I ' I ' ' ' ' I ' I M I I I . I I I I I I I r Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00
LBD.D NP091101.M Tue Oct 02 12:28:45 2001 Page 11
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NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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