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GC/MS calibration table for TCLP analytes, October 2001

Machine-extracted title · confidence 90%

Calibration data table for TCLP analysis including retention times and response factors for various compounds.

NYC-WTC_000086981–000087006

Folder label: “508 Scan 9/17/01 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0101\LBD.D Vial: 4 Acq On ; 1 Oct 2001 4:39 pm Operator: 2 09 GTVLOS Sample ; 9/17 Inst : GC/MS 209 Mise Multiplr: 1,00 MS Integration Params; LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Octadecane Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 30.74 1.49 ug/1 231479 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane 254 C18H38 000593-45-3 91 2 Tetracosane 338 C24H50 000646-31-1 90 3 Tricosane 324 C23H48 000638-67-5 90 4 Eicosane 282 C20H42 000112-95-8 90 Abundance Scan 2799 (30.738 min); LBD.D (-) m/z 57.00 100.00% 57 71 43 85 5000-

99 ‘T 30.40 30.60 30.80 31.00 ,A,4,,, I................, m/z 71.10 77714% ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71561: Octadecane 43 71

85 5000- 30.40 30.60 30.80 31.00 99 m/z 43.00 64.96% I I .1 . I I I 1 r I { r \ I I | I I I I I I I ■ ■ I I I I I I ■ I I I I I I I > I I < Bl I I I I I I I I . . I < I I I I I I I I | i mte-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance 43 57 71 #73543: Tetracosane

. n.. 30.40 30.60 30.80 31.00 5000 85 m/z 85.05 51.98%

99 in J I L J T? ■I ' ' ' H ' ' ' 155169183197 T p •' ’ I 294 I'''' I 338 I'''' I * n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73318: Tricosane 43 57 30.40 30.60 30.80 31.00 m/z 41.05 28.26% 71 5000 85

Tl/Z~> T-rp-T 40 ,, L80Ji , ,T.100 120 140 .160 ........ 60 . 180 200 220 240 260 280 3^ 320 340 30.40 30.60 30.80 31.00

LBD.D NP091101.M Tue Oct 02 12:28:41 2001 Page 10

NYC-WTC_000086996

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NYC-WTC_000086996Source: NYC Law Department, mirrored locally

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